Synthesis of Ether-free Organomagnesium Compounds

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Description

At the time this work was begun, there was some confusion about the technique necessary for the successful synthesis of organomagnesium compounds in hydrocarbon solvents and without solvents. It was decided to repeat the work of Bryce-Smith and Zakharkin. Thus began the study of the synthesis of organomagnesium compounds without solvents; the study of the reaction products of these organomagnesium compounds in hydrocarbons plus 2-butanone compared to the reaction products of the corresponding etheral Grignard reagent plus 2-butanone; and a preliminary study of the nature of these organomagnesium compounds in hydrocarbon solvents.

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iv, 43 leaves : ill.

Creation Information

Hanicak, John E. August 1967.

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  • Hanicak, John E.

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Description

At the time this work was begun, there was some confusion about the technique necessary for the successful synthesis of organomagnesium compounds in hydrocarbon solvents and without solvents. It was decided to repeat the work of Bryce-Smith and Zakharkin. Thus began the study of the synthesis of organomagnesium compounds without solvents; the study of the reaction products of these organomagnesium compounds in hydrocarbons plus 2-butanone compared to the reaction products of the corresponding etheral Grignard reagent plus 2-butanone; and a preliminary study of the nature of these organomagnesium compounds in hydrocarbon solvents.

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iv, 43 leaves : ill.

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UNT Theses and Dissertations

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  • August 1967

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  • Dec. 27, 2012, 10:03 p.m.

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  • Sept. 5, 2013, 3:35 p.m.

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Hanicak, John E. Synthesis of Ether-free Organomagnesium Compounds, thesis, August 1967; Denton, Texas. (https://digital.library.unt.edu/ark:/67531/metadc130849/: accessed May 26, 2019), University of North Texas Libraries, Digital Library, https://digital.library.unt.edu; .