Noise reduction in negative-ion quadrupole mass spectrometry Page: 4 of 22
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Mass spectrometers can accurately measure even very small
concentrations of ions, and thus are useful tools for chemical analysis.
Specialized techniques based on mass spectrometry include secondary
ion mass spectrometry (SIMS), Auger spectroscopy, electron
5 scattering for chemical analysis (ESCA), ion probe mass spectrometry,
and inductively coupled plasma (ICP) mass spectrometry. Mass
spectrometers can also be used as leak detectors and residual gas
analyzers.
A mass spectrometer includes three basic components: an ion
10 source, which produces a beam of ionized particles from a sample; a
means for separating different ion types in the beam by e/m ratio; and
a detector, which measures and records the intensity of each of the
types.
Many different ion sources are available. For example, gas
15 samples may be ionized by an electron beam in an ionization chamber;
solid or liquid samples may be vaporized by a laser beam, resulting in
ejection of neutral atoms and charged particles that form a plasma;
actinide samples may be obtained by using thermal ionization
filaments. Recent developments include ion production by inductively
20 coupled plasma torches, fast atom bombardment of liquid surfaces,
and ionizing the surface molecules of a liquid sample with weak laser
light. In a typical mass spectrometer, ions exiting the source are
formed into a beam and accelerated by an electric potential V before
entering the magnetic field where they are separated according to their
25 mass and charge. The radius of curvature of the path of an ion with
mass m and charge e in a magnetic field H is
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Chastagner, P. Noise reduction in negative-ion quadrupole mass spectrometry, patent, December 31, 1991; Aiken, South Carolina. (https://digital.library.unt.edu/ark:/67531/metadc1281515/m1/4/: accessed April 23, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.