Determination of the Formation Constant of Indiumacetylacetonate by an Extraction Method

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Description

1. The solubility of acetylacetone has been determined in an acetate buffer solution of ionic strength C.1 in relation to pH and temperature. 2. The distribution coefficients of acetylacetone have been determined between chloroform, carbon tetrachloride, benzene and an acetate buffer solution in relation to acetylacetone concentration and pH. 3. The relationship has been established between the rate at which indium acetylacetonate reaches partition equilibrium and the pH, initial acetylacetone concentration in the organic phase, and the different organic solvents. 4. The extent of the extraction of indiumacetylacetonate has been determined for three organic solvents at two acetylacetone concentrations in … continued below

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19 pages : illustrations

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Rudenko, N. P. (Nikolaĭ Petrovich); Stary, I. & de Bruin, H. J. 1959.

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  • Main Title: Determination of the Formation Constant of Indiumacetylacetonate by an Extraction Method
  • Added Title: AAEC/Trans. (Lucas Heights, N.S.W.)
  • Series Title: Australian Atomic Energy Commission Reports
  • Added Title: Australian Atomic Energy Commission Report TRANS-1

Description

1. The solubility of acetylacetone has been determined in an acetate buffer solution of ionic strength C.1 in relation to pH and temperature. 2. The distribution coefficients of acetylacetone have been determined between chloroform, carbon tetrachloride, benzene and an acetate buffer solution in relation to acetylacetone concentration and pH. 3. The relationship has been established between the rate at which indium acetylacetonate reaches partition equilibrium and the pH, initial acetylacetone concentration in the organic phase, and the different organic solvents. 4. The extent of the extraction of indiumacetylacetonate has been determined for three organic solvents at two acetylacetone concentrations in relation of pH. The independence of the degree of extraction from indium concentration was established in the region between 10(-4) to 10(-6) M. 5. 5. The indium acetylacetone compound was obtained by extraction from organic solvents. 6. The stability constants were calculated by two different methods for the uncharged complex and intermediate complexes; also the constants for the various steps of the dissociation of indiumacetylacetonate.

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19 pages : illustrations

Notes

Digitized from microopaque cards (1).

Translated from Trudy Komissii Po Analiticheskoy Khimii, (Academy of Sciences of U.S.S.R.), (Vol. IX (XII), pp 28-43 (1958)).

Includes bibliographic refences (page 12).

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  • SuDoc Number: Y 3.At 7:22/AAEC/TRANS-1
  • Report No.: AAEC/Trans-1
  • Accession or Local Control No: metadc1257825
  • Archival Resource Key: ark:/67531/metadc1257825

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  • 1959

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  • June 18, 2021, 7:31 a.m.

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  • May 24, 2023, 12:47 p.m.

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Rudenko, N. P. (Nikolaĭ Petrovich); Stary, I. & de Bruin, H. J. Determination of the Formation Constant of Indiumacetylacetonate by an Extraction Method, report, 1959; Lucas Heights, New South Wales, Australia. (https://digital.library.unt.edu/ark:/67531/metadc1257825/: accessed May 19, 2025), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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