The Preparation of High-Purity Beryllium Oxide

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Description

Abstract. A method for the preparation of beryllium oxide of high purity is presented. Beryllium basic acetate (BeO-3Be(C2H3O2)2) is prepared from the metal or a convenient salt, a chloroform solution of this material extracted with redistilled water, the dried basic acetate distilled in a quartz apparatus, and this purified material converted to the oxide by fuming down with sulfuric acid and igniting at 1000 degrees C. Impurities detectable spectrographically were reduced to a very low level.

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5 pages : illustrations

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Tomkins, F. S.; Cressman, G. W. & Tolmach, L. J. May 27, 1946.

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Description

Abstract. A method for the preparation of beryllium oxide of high purity is presented. Beryllium basic acetate (BeO-3Be(C2H3O2)2) is prepared from the metal or a convenient salt, a chloroform solution of this material extracted with redistilled water, the dried basic acetate distilled in a quartz apparatus, and this purified material converted to the oxide by fuming down with sulfuric acid and igniting at 1000 degrees C. Impurities detectable spectrographically were reduced to a very low level.

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5 pages : illustrations

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Digitized from microopaque cards (1).

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  • SuDoc Number: Y 3.At 7:22/CC-3524
  • Report No.: CC-3524
  • Accession or Local Control No: metadc1256416
  • Archival Resource Key: ark:/67531/metadc1256416

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  • May 27, 1946

Added to The UNT Digital Library

  • Aug. 10, 2021, 7:39 a.m.

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  • Jan. 26, 2022, 12:54 p.m.

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Tomkins, F. S.; Cressman, G. W. & Tolmach, L. J. The Preparation of High-Purity Beryllium Oxide, report, May 27, 1946; Washington D.C.. (https://digital.library.unt.edu/ark:/67531/metadc1256416/: accessed September 4, 2026), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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