Characterization of Phenolic Resins With Thermogravimetry-Mass Spectrometry

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As part of an advanced material research program, thermogravimetry-mass spectrometry (TG-MS) analysis of a phenolic resin was carried out recently for the study of the curing of the prepolymer, solvent extraction, and carbonization of the polymer at high temperature in inert atmosphere. These steps are critical to the quality of the produced advanced material. In addition to TG-MS, several other complementary techniques were also employed for the analysis of the phenolic resin prepolymer and its curing and thermal degradation products. These techniques include pyrolysis-gas chromatography-mass spectrometry, direct insertion probe-mass spectrometry and gas chromatography-mass spectrometry. 7 refs., 5 figs., 3 tabs.

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12 pages

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Chang, Cherng & Tackett, Juanita R. January 1, 1990.

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This article is part of the collection entitled: Office of Scientific & Technical Information Technical Reports and was provided by the UNT Libraries Government Documents Department to the UNT Digital Library, a digital repository hosted by the UNT Libraries. It has been viewed 120 times. More information about this article can be viewed below.

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Description

As part of an advanced material research program, thermogravimetry-mass spectrometry (TG-MS) analysis of a phenolic resin was carried out recently for the study of the curing of the prepolymer, solvent extraction, and carbonization of the polymer at high temperature in inert atmosphere. These steps are critical to the quality of the produced advanced material. In addition to TG-MS, several other complementary techniques were also employed for the analysis of the phenolic resin prepolymer and its curing and thermal degradation products. These techniques include pyrolysis-gas chromatography-mass spectrometry, direct insertion probe-mass spectrometry and gas chromatography-mass spectrometry. 7 refs., 5 figs., 3 tabs.

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12 pages

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NTIS, PC A03/MF A01 - OSTI; GPO Dep.

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  • 19. annual North American thermal analysis society conference, Boston, MA (USA), 23-26 Sep 1990

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  • Other: DE91002710
  • Report No.: MLM-3668(OP)
  • Report No.: CONF-9009223--4
  • Grant Number: AC04-88DP43495
  • Office of Scientific & Technical Information Report Number: 6333297
  • Archival Resource Key: ark:/67531/metadc1210141

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Office of Scientific & Technical Information Technical Reports

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  • January 1, 1990

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  • July 5, 2018, 11:11 p.m.

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  • April 29, 2019, 1:32 p.m.

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Chang, Cherng & Tackett, Juanita R. Characterization of Phenolic Resins With Thermogravimetry-Mass Spectrometry, article, January 1, 1990; United States. (https://digital.library.unt.edu/ark:/67531/metadc1210141/: accessed April 23, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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