Characterization of high boiling fossil fuel distillates via /sup 1/H and /sup 13/C NMR analysis. Quarterly report II, October 1, 1978--December 31, 1978

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The goals reached in the second quarter of the original contract are the completion of the /sup 1/H NMR analysis of all of the concentrates (monoaromatic, diaromatic, polyaromatic-polar and saturates) and GPC (gel permeation chromatography) fractions 211-76 No. 16 and 24 (diaromatic) and 210-76 No. 16, 21 and 26 (polyaromatic-polar) distillates (535 to 670/sup 0/C) of Wilmington crude and the concentrates and GPC fractions 207-76 No. 15 and 24 (diaromatic) and 208-76 No. 15, 20 and 25 (polyaromatic-polar) of Gach Saran crude. In addition, the /sup 13/C NMR analysis was completed of the monoaromatic GPC fractions of Wilmington (209-76 No. ... continued below

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Pages: 63

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Berlin, K.D.; O'Donnell, D.J. & Sigle, S. January 1, 1978.

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Description

The goals reached in the second quarter of the original contract are the completion of the /sup 1/H NMR analysis of all of the concentrates (monoaromatic, diaromatic, polyaromatic-polar and saturates) and GPC (gel permeation chromatography) fractions 211-76 No. 16 and 24 (diaromatic) and 210-76 No. 16, 21 and 26 (polyaromatic-polar) distillates (535 to 670/sup 0/C) of Wilmington crude and the concentrates and GPC fractions 207-76 No. 15 and 24 (diaromatic) and 208-76 No. 15, 20 and 25 (polyaromatic-polar) of Gach Saran crude. In addition, the /sup 13/C NMR analysis was completed of the monoaromatic GPC fractions of Wilmington (209-76 No. 15 and 23) and Gach Saran (Concentrate and 206-76 No. 14, 18 and 22) distillates as well as the /sup 13/C NMR analysis of the concentrates of the diaromatic, polyaromatic-polar and saturate fractions of Wilmington and Gach Saran distillates. The acquisition of /sup 13/C NMR spectra of the remaining fractions is steadily progressing, although long acquisition times (for example, 63 hours per spectrum) will slow somewhat the rate at which data can be obtained.

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Pages: 63

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Dep. NTIS, PC A04/MF A01.

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  • Report No.: BETC-001-2
  • Grant Number: EW-78-S-19-0001
  • DOI: 10.2172/6364763 | External Link
  • Office of Scientific & Technical Information Report Number: 6364763
  • Archival Resource Key: ark:/67531/metadc1205211

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  • January 1, 1978

Added to The UNT Digital Library

  • July 5, 2018, 11:11 p.m.

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  • Sept. 5, 2018, 2:20 p.m.

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Berlin, K.D.; O'Donnell, D.J. & Sigle, S. Characterization of high boiling fossil fuel distillates via /sup 1/H and /sup 13/C NMR analysis. Quarterly report II, October 1, 1978--December 31, 1978, report, January 1, 1978; United States. (digital.library.unt.edu/ark:/67531/metadc1205211/: accessed December 10, 2018), University of North Texas Libraries, Digital Library, digital.library.unt.edu; crediting UNT Libraries Government Documents Department.