Analysis of Mixtures of Alcohols by Acylation

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Description

From abstract: "Recently a general chemical method for the analysis of mixtures of alcohols appeared, using pyridine catalyzed acetylation and second order kinetics to determine the amount of the faster reacting component. The use of 0.25M isobutyric anhydride in pyridine containing 0.0025M perchloric acid as catalyst promotes the rate of the reaction and diminishes the time necessary to perform an analysis. A mathematical treatment of the data and kinetic plot reduces the number of kinetic points to only four or five. The mixtures are primarily composed of isomers."

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v, 33 pages : illustrations.

Creation Information

Fellows, William Dean & Fritz, James S. (James Sherwood), 1924- November 1961.

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This report is part of the collection entitled: Technical Report Archive and Image Library and was provided by the UNT Libraries Government Documents Department to the UNT Digital Library, a digital repository hosted by the UNT Libraries. It has been viewed 11 times. More information about this report can be viewed below.

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  • Ames Laboratory
    Publisher Info: Ames Laboratory, Iowa State University.
    Place of Publication: Ames, Iowa

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Description

From abstract: "Recently a general chemical method for the analysis of mixtures of alcohols appeared, using pyridine catalyzed acetylation and second order kinetics to determine the amount of the faster reacting component. The use of 0.25M isobutyric anhydride in pyridine containing 0.0025M perchloric acid as catalyst promotes the rate of the reaction and diminishes the time necessary to perform an analysis. A mathematical treatment of the data and kinetic plot reduces the number of kinetic points to only four or five. The mixtures are primarily composed of isomers."

Physical Description

v, 33 pages : illustrations.

Notes

Digitized from microopaque cards.

"Chemistry."

"November, 1961."

"F. H. Spedding, Director, Ames Laboratory."

"Work performed under Contract No. W-7405-Eng-82."

"This report is based on a Ph.D. thesis by William Dean Fellows submitted November, 1961, to Iowa State University, Ames, Iowa. This work was done under contract with the U.S. Atomic Energy Commission."

Includes bibliographical references (page 30).

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  • Report No.: IS-510
  • SuDoc Number: Y 3.At 7:22/IS-510
  • Accession or Local Control No: metadc1201526
  • Grant Number: W-7405-Eng-82
  • Archival Resource Key: ark:/67531/metadc1201526

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Technical Report Archive and Image Library

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Imaged from microcard, these technical reports describe research performed for U.S. government agencies from the 1930s to the 1960s. The reports were provided by the Technical Report Archive and Image Library (TRAIL).

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  • November 1961

Added to The UNT Digital Library

  • Aug. 27, 2019, 3:53 p.m.

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  • April 1, 2020, 3:24 p.m.

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Fellows, William Dean & Fritz, James S. (James Sherwood), 1924-. Analysis of Mixtures of Alcohols by Acylation, report, November 1961; Ames, Iowa. (https://digital.library.unt.edu/ark:/67531/metadc1201526/: accessed April 23, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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