Organic Reactor Technology Quarterly Report, April 1-June 30, 1962
Description
The deposition of film was studied in irradiated circulating loops, in which both grounded and insulated plates were in the irradiated coolant volume; the purpose of these tests was to determine the effect on rate of film formation of charges generated on particulate matter or coolant molecules in the radiation field. Heavier deposits were found on the grounded plates and currents up to 30 microamp were measured flowing to this plate. Tests in the rocking cell showed that techniques are now available whereby this apparatus can be used with confidence to screen film-forming characteristics of coolant compositions. It was demonstrated … continued below
Physical Description
107 pages
Creation Information
Creator: Unknown. October 15, 1962.
Context
This report is part of the collection entitled: Office of Scientific & Technical Information Technical Reports and was provided by the UNT Libraries Government Documents Department to the UNT Digital Library, a digital repository hosted by the UNT Libraries. It has been viewed 26 times. More information about this report can be viewed below.
Who
People and organizations associated with either the creation of this report or its content.
Creator
- We've been unable to identify the creator(s) of this report.
Publisher
-
Phillips Petroleum Company. Atomic Energy Division.
Publisher Info: Phillips Petroleum Co. Atomic Energy Div., Idaho Falls, IdahoPlace of Publication: Idaho Falls, Idaho
Provided By
UNT Libraries Government Documents Department
Serving as both a federal and a state depository library, the UNT Libraries Government Documents Department maintains millions of items in a variety of formats. The department is a member of the FDLP Content Partnerships Program and an Affiliated Archive of the National Archives.
Contact Us
What
Descriptive information to help identify this report. Follow the links below to find similar items on the Digital Library.
Titles
- Main Title: Organic Reactor Technology Quarterly Report, April 1-June 30, 1962
- Serial Title: INEL Organic Reactor Technology Progress Report
Description
The deposition of film was studied in irradiated circulating loops, in which both grounded and insulated plates were in the irradiated coolant volume; the purpose of these tests was to determine the effect on rate of film formation of charges generated on particulate matter or coolant molecules in the radiation field. Heavier deposits were found on the grounded plates and currents up to 30 microamp were measured flowing to this plate. Tests in the rocking cell showed that techniques are now available whereby this apparatus can be used with confidence to screen film-forming characteristics of coolant compositions. It was demonstrated that iron percarbide (Fe/sub 20/C/sub 9/) could be made under conditions comparable to those in the OMRE. It was made from an iron chelate by carbon monoxide reduction and emphasizes the possible importance of oxygen containing chelate in the transport of iron and deposition of film. The nature of the impurities occurring in commercial Santowax was examined and some highly colored, oxygenated material isolated. The hexaphenyls produced in irradiation of m- and p-terphenyls and in the reaction of polyphenyls with hydrogen atoms was studied. Further work was initiated in the area of synthesis of reference hexaphenyls, but synthesis of new candidate coolants also was continued. Areas under study included non-benzenoid heterocyclics, fused ring compounds, and hydrogen donor compounds. Partially hydrogenated fused ring structures, such as dihydrophenanthrene, continue to look very promising. Stabilizer studies were directed largely toward this area also, but the stabilizer program was brought to a close. The study of hydrocracking of high boiler was completed with a few additional catalyst tests. The treatment of unfractionated coolant was further developed and cortinued to look like the most desirable operation. Preliminary economic evaluations on the hydrocracking routes to reclamation were completed and looked attractive. Design liaison on the coolant technology and fuel technology loops and on loop handling equipment is nearing completion. Loop construction is about 13% completed. Overall completion of the basic EOCR was approximately 90% at the end of the reporting period. The outof-pile Component Developmert Test Loop was operated for chem-pump testing with diphenyl-terphenyl eutectic fluid at temperatures up to 600 deg F. Methods of attaching thermocouples to fuel plates and of leading them out of the fuel assembly were studied. Both high temperature furnace brazing and resistance spot welding were used for attachment in these studies, and the brazing method was selected as the preferred method for attaching thermocouples to the instrumerted fuel plates. A detailed study of the locations of the thermocouples was completed. The practicability of using ethylene glycol as a displacement cleaner of fuel elements was demonstrated. Studies on film formation from Santowax refluxed with chemically cleaned pipe sections indicated that the passivation film dissolves in the organlc and increases the film deposit. this effect is eliminated by one refluxing with Santowax. Capsules for use in the MTR hydraulic rabbit facility were designed and built. These furnish heat by gamma absorption and permit organic samples to be irradiated at desired temperatures in a neutron field. An improved capsule for pyrolytic fouling was under test. Initial results were satisfactory and indicate that useful heat transfer data on the coolant may be an unexpected dividend from use of this apparatus. (auth)
Physical Description
107 pages
Notes
Other Information: Orig. Receipt Date: 31-DEC-63
Subjects
Keywords
- Absorption
- Alcohols
- Aromatics
- Brazing
- Cables
- Capsules
- Carbon Monoxide
- Catalysis
- Chelates
- Chemical Reactions
- Cleaning
- Coolant Loops
- Decomposition
- Economics
- Electric Conductivity
- Electrodes
- Eocr
- Ethylene
- Eutectics
- Films
- Fluids
- Fuel Elements
- Fuels
- Gamma Radiation
- Glycols
- Heat Transfer
- Heating
- Heterocyclics
- High Temperature
- Hydraulics
- Hydrogen
- Impurities
- In Pile Loops
- Iron
- Iron Carbides
- Irradiation
- Laboratory Equipment
- Layers
- Materials Testing
- Mockup
- Molecules
- Mtr
- Neutron Flux
- Omre
- Operation
- Organic Compounds
- Organic Coolant
- Organic Sulfur Compounds
- Oxides
- Oxygen
- Passivation
- Phenanthrene
- Pipes
- Reactor Technology
Language
Item Type
Identifier
Unique identifying numbers for this report in the Digital Library or other systems.
- Report No.: IDO-16807
- Grant Number: AT(10-1)-205
- Digital Object Identifier: https://doi.org/10.2172/4730000
- Office of Scientific & Technical Information Report Number: 4730000
- Archival Resource Key: ark:/67531/metadc1030075
Collections
This report is part of the following collection of related materials.
Office of Scientific & Technical Information Technical Reports
Reports, articles and other documents harvested from the Office of Scientific and Technical Information.
Office of Scientific and Technical Information (OSTI) is the Department of Energy (DOE) office that collects, preserves, and disseminates DOE-sponsored research and development (R&D) results that are the outcomes of R&D projects or other funded activities at DOE labs and facilities nationwide and grantees at universities and other institutions.
Digital Files
When
Dates and time periods associated with this report.
Creation Date
- October 15, 1962
Added to The UNT Digital Library
- Oct. 18, 2017, 7:39 a.m.
Description Last Updated
- Nov. 22, 2024, 9:51 p.m.
Usage Statistics
When was this report last used?
Interact With This Report
Here are some suggestions for what to do next.
Citations, Rights, Re-Use
International Image Interoperability Framework

We support the IIIF Presentation API
Print / Share
Links for Robots
Helpful links in machine-readable formats.
Archival Resource Key (ARK)
- ERC Record: /ark:/67531/metadc1030075/?
- Persistence Statement: /ark:/67531/metadc1030075/??
International Image Interoperability Framework (IIIF)
- IIIF Manifest: /ark:/67531/metadc1030075/manifest/
Metadata Formats
- UNTL Format: /ark:/67531/metadc1030075/metadata.untl.xml
- DC RDF: /ark:/67531/metadc1030075/metadata.dc.rdf
- DC XML: /ark:/67531/metadc1030075/metadata.dc.xml
- OAI_DC: /oai/?verb=GetRecord&metadataPrefix=oai_dc&identifier=info:ark/67531/metadc1030075
- METS: /ark:/67531/metadc1030075/metadata.mets.xml
- OpenSearch Document: /ark:/67531/metadc1030075/opensearch.xml
Images
- Thumbnail: /ark:/67531/metadc1030075/thumbnail/
- Small Image: /ark:/67531/metadc1030075/small/
URLs
- In-text: /ark:/67531/metadc1030075/urls.txt
Stats
- Usage Stats: /stats/stats.json?ark=ark:/67531/metadc1030075
Organic Reactor Technology Quarterly Report, April 1-June 30, 1962, report, October 15, 1962; Idaho Falls, Idaho. (https://digital.library.unt.edu/ark:/67531/metadc1030075/: accessed July 18, 2025), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.