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Synthesis and Characterization of 2,3-Dichloropyrrolo[1,2-a]benzimidazol-1-one and Its Methylthiol Derivatives

Description: Condensation of 2,3-dichloromaleic anhydride and o-phenylenediamine in refluxing toluene affords the three compounds 2,3-dichloro-N-o-C6H4(NH2)maleimide (1), N,N¢-o-C6H4-bis(2,3-dichloromaleimide) (2), and 2,3-dichloropyrrolo[1,2-a]benzimidazol-1-one (3), with compound 1 as the major product. Repeating the same reaction in the presence of added PTSA furnishes compound 3 as the major product. Treatment of 3 with methylthiol in the presence of pyridine affords monosulfide compounds 2-chloro-3-met… more
Date: May 2006
Creator: Wu, Guanmin
Partner: UNT Libraries
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Sulfur Compounds in Crude Oil

Description: From Abstract: "This report summarizes a systematic 20-year study of the organic sulfur compounds in Wasson, Texas, crude oil and, to a lesser extent, of three crude oils, that culminated in some 200 individual sulfur-compound identifications. This report reviews early sulfur literature covering petroleum sulfur compound identifications completed before this study was begun, and cites 58 papers resulting from this work."
Date: 1972
Creator: Rall, H. T.; Thompson, C. J.; Coleman, H. J. & Hopkins, R. L.
Partner: UNT Libraries Government Documents Department
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