Orientation, Microstructure and Pile-Up Effects on Nanoindentation Measurements of FCC and BCC Metals

Orientation, Microstructure and Pile-Up Effects on Nanoindentation Measurements of FCC and BCC Metals

Date: May 2008
Creator: Srivastava, Ashish Kumar
Description: This study deals with crystal orientation effect along with the effects of microstructure on the pile-ups which affect the nanoindentation measurements. Two metal classes, face centered cubic (FCC) and body centered cubic (BCC, are dealt with in the present study. The objective of this study was to find out the degree of inaccuracy induced in nanoindentation measurements by the inherent pile-ups and sink-ins. Also, it was the intention to find out how the formation of pile-ups is dependant upon the crystal structure and orientation of the plane of indentation. Nanoindentation, Nanovision, scanning electron microscopy, electron dispersive spectroscopy and electron backscattered diffraction techniques were used to determine the sample composition and crystal orientation. Surface topographical features like indentation pile-ups and sink-ins were measured and the effect of crystal orientation on them was studied. The results show that pile-up formation is not a random phenomenon, but is quite characteristic of the material. It depends on the type of stress imposed by a specific indenter, the depth of penetration, the microstructure and orientation of the plane of indentation. Pile-ups are formed along specific directions on a plane and this formation as well as the pile-up height and the contact radii with the indenter ...
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Mechanical Characterization of A2 and D2 Tool Steels By Nanoindentation

Mechanical Characterization of A2 and D2 Tool Steels By Nanoindentation

Date: May 2012
Creator: Okafor, Uzochukwu Chimezie
Description: Nanoindentation technique was used to investigate the surface properties of A2 and D2 tool steel subjected to different heat treatments. the mechanical characteristics of these two easily available tool steels were studied based on microstructural images obtained from SEM, the grain growth after heat treatment using X-ray diffraction method and nanoindentation technique. the investigation showed that a single nanoindentation result can explain how heat treatment influences reliability and failure in A2 and D2 tool steels. in this work, the causes and effects of these variations were studied to explain how they influence reliability and failure in A2 and D2 tool steel. Finally, a cube-corner indenter tip was used to determine the fracture toughness of silicon wafer. the emphasis of this research is on how nanoindentation technique is more extensive in material characterization.
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Laminar Natural Convection From Isothermal Vertical Cylinders

Laminar Natural Convection From Isothermal Vertical Cylinders

Date: August 2012
Creator: Day, Jerod
Description: Laminar natural convection heat transfer from the vertical surface of a cylinder is a classical subject, which has been studied extensively. Furthermore, this subject has generated some recent interest in the literature. In the present investigation, numerical experiments were performed to determine average Nusselt numbers for isothermal vertical cylinders (103 < RaL < 109, 0.5 < L/D <10, and Pr = 0.7) with and without an adiabatic top in a quiescent ambient environment which will allow for plume growth. Results were compared with commonly used correlations and new average Nusselt number correlations are presented. Furthermore, the limit for which the heat transfer results for a vertical flat plate may be used as an approximation for the heat transfer from a vertical cylinder was investigated.
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Mist Characterization in Drilling 1018 Steel

Mist Characterization in Drilling 1018 Steel

Date: August 2012
Creator: Cole, Ian
Description: Minimum quantity lubrication replaces the traditional method of flood cooling with small amounts of high-efficient lubrication. Limited studies have been performed to determine the characteristics of mist produced during MQL. This study investigated the mist concentration levels produced while drilling 1018 steel using a vegetable based lubricant. ANOVA was performed to determine whether speed and feed rates or their interactions have a significant effect on mist concentration levels and particle diameter. It was observed that the concentration levels obtained under all four speed and feed rate combinations studied exceeded the current OSHA and NIOSH standards.
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Indentation induced deformation in metallic materials.

Indentation induced deformation in metallic materials.

Date: December 2005
Creator: Vadlakonda, Suman
Description: Nanoindentation has brought in many features of research over the past decade. This novel technique is capable of producing insights into the small ranges of deformation. This special point has brought a lot of focus in understanding the deformation behavior under the indenter. Nickel, iron, tungsten and copper-niobium alloy system were considered for a surface deformation study. All the samples exhibited a spectrum of residual deformation. The change in behavior with indentation and the materials responses to deformation at low and high loads is addressed in this study. A study on indenter geometry, which has a huge influence on the contact area and subsequently the hardness and modulus value, has been attempted. Deformation mechanisms that govern the plastic flow in materials at low loads of indentation and their sensitivity to the rate of strain imparted has been studied. A transition to elastic, plastic kind of a tendency to an elasto-plastic tendency was seen with an increase in the strain rate. All samples exhibited the same kind of behavior and a special focus is drawn in comparing the FCC nickel with BCC tungsten and iron where the persistence of the elastic, plastic response was addressed. However there is no absolute reason ...
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Interspecimen Study of Bone to Relate Macromechanical, Nanomechanical and Compositional Changes Across the Femoral Cortex of Bone

Interspecimen Study of Bone to Relate Macromechanical, Nanomechanical and Compositional Changes Across the Femoral Cortex of Bone

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Date: May 2013
Creator: Nar, Mangesh
Description: Mechanics of bone is widely studied and researched, mainly for the study of fracture. This has been done mostly on a macro scale. In this work hierarchical nature of bone has been explored to investigate bone mechanics in more detail. Flexural test were done to classify the bones according to their strength and deflection. Raman spectroscopy analysis was done to map the mineralization, collagen crosslinking changes across the thickness of the bone. Nanoindentation was done to map indentation hardness and indentation modulus across femoral cortex of the bone. The results indicate that the composition of the bone changes across the thickness of the femoral cortex. The hypothesis is confirmed as increase in mineralization, carbonate to phosphate ratio and collagen crosslinking shows the effect as increased indentation hardness and modulus and decreased deflection.
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Analytical Model of Cold-formed Steel Framed Shear Wall with Steel Sheet and Wood-based Sheathing

Analytical Model of Cold-formed Steel Framed Shear Wall with Steel Sheet and Wood-based Sheathing

Date: May 2013
Creator: Yanagi, Noritsugu
Description: The cold-formed steel framed shear walls with steel sheets and wood-based sheathing are both code approved lateral force resisting system in light-framed construction. In the United States, the current design approach for cold-formed steel shear walls is capacity-based and developed from full-scale tests. The available design provisions provide nominal shear strength for only limited wall configurations. This research focused on the development of analytical models of cold-formed steel framed shear walls with steel sheet and wood-based sheathing to predict the nominal shear strength of the walls at their ultimate capacity level. Effective strip model was developed to predict the nominal shear strength of cold-formed steel framed steel sheet shear walls. The proposed design approach is based on a tension field action of the sheathing, shear capacity of sheathing-to-framing fastener connections, fastener spacing, wall aspect ratio, and material properties. A total of 142 full scale test data was used to verify the proposed design method and the supporting design equations. The proposed design approach shows consistent agreement with the test results and the AISI published nominal strength values. Simplified nominal strength model was developed to predict the nominal shear strength of cold-formed steel framed wood-based panel shear walls. The nominal shear ...
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Effect of Amines as Corrosion Inhibitors for a Low Carbon Steel in Power Industry

Effect of Amines as Corrosion Inhibitors for a Low Carbon Steel in Power Industry

Date: December 2004
Creator: Díaz, Jorge G.
Description: Commonly used amines in power industry, including morpholine, DBU (1,8-diazabicyclo[5.4.0]undec-7-ene), and DMA (dimethylallylamine) were evaluated for their effect on AISI 1018 steel at 250oF. Samples were exposed to an autoclave containing amine added aqueous solution at pH of 9.5 for 1, 2, 4, 6, 8, and 12 hours. Morphology studies were carried using scanning electron microscope (SEM), phase analysis was done utilizing Fourier transform infrared spectroscopy (FTIR), and weight loss was performed to assess kinetics of oxidation. Control samples showed the highest metal dissolution rate. DBU showed the best performance in metal protection and SEM indicated the presence of a free-crack layer formed by fine particles in that set. FTIR showed that DBU apparently favored the formation of magnetite. It is believed that fine particles impede intrusion of aggressive ions into the metal surface by forming a barrier layer. FTIR demonstrated that DMA formed more oxyhydroxides, whereas morpholine presented magnetite to hematite transformation as early as 2 hours. SEM revealed that control and DMA produced acicular particles characteristic of oxyhydroxides while morpholine and DBU presented more equiaxed particles.
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Effects of Thickness and Indenter Tip Geometry in Nanoindentation of Nickel Films

Effects of Thickness and Indenter Tip Geometry in Nanoindentation of Nickel Films

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Date: May 2004
Creator: Parakala, Padma
Description: Nanoindentation has become a widely used technique to measure the mechanical properties of materials. Due to its capability to deform materials in micro- and nano-scale, nanoindentation has found more applications in characterizing the deformation behavior and determining the mechanical properties of thin films and coatings. This research deals with the characterization of samples received from Center for Advanced Microstructures and Devices (CAMD) and Integran Technologies Inc., Toronto, Canada and the objective of this investigation was to utilize the experimental data obtained from nanoindentation to determine the deformation behavior, mechanical properties of thin films on substrates and bulk materials, and the effect of geometrically different indenters (Berkovich, cubecorner, and conical). X-ray diffraction (XRD), transmission electron microscope (TEM), scanning electron microscopy (SEM), and atomic force microscopy (AFM) analysis were performed on these materials to determine the crystal orientation, grain size of the material, and also to measure any substrate effects like pile-up or sin-in respectively. The results indicate that indentation size effect (ISE) strongly depends on shape of the indenter and less sensitive to penetration depth where as the hardness measurements depends on shape of indenter and depth of penetration. There is a negligible strain rate dependency of hardness at deeper depths ...
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Effects of Rebar Temperature and Water to Cement Ratio on Rebar-Concrete Bond Strength of Concrete Containing Fly Ash

Effects of Rebar Temperature and Water to Cement Ratio on Rebar-Concrete Bond Strength of Concrete Containing Fly Ash

Date: May 2010
Creator: Pati, Ardeep Ranjan
Description: This research presents the results on an experimental investigation to identify the effects of rebar temperature, fly ash and water to cement ratio on concrete porosity in continuously reinforced concrete pavements (CRCP). Samples were cast and analyzed using pullout tests. Water to cement ratio (w/c) and rebar temperature had a significant influence on the rebar-concrete bond strength. The 28-day shear strength measurements showed an increase in rebar-concrete bond strength as the water to cement ratio (w/c) was reduced from 0.50 to 0.40 for both fly ash containing and non fly ash control samples. There was a reduction in the peak pullout load as the rebar surface temperature increased from 77o F to 150o F for the cast samples. A heated rebar experiment was performed simulating a rebar exposed to hot summer days and the rebar cooling curves were plotted for the rebar temperatures of 180o F - 120o F. Fourier transform infrared spectroscopy was performed to show the moisture content of cement samples at the rebar-concrete interface. Mercury intrusion porosimetry test results on one batch of samples were used for pore size distribution analysis. An in-depth analysis of the morphological characteristics of the rebar-concrete interface and the observation of pores ...
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