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Consolidation and shaping of boron ; summary of previous work

Description: From abstract: "The deposit on the rods is in the form of a brittle uneven tube which is cracked off and subsequently pulverized to a 200-mesh powder. This report is chiefly concerned with methods of consolidating this powder and shaping it into forms required, though it also discusses to some extent other methods of shaping boron or born-rich materials."
Date: October 8, 1945
Creator: Kamm, Robert L.
Partner: UNT Libraries Government Documents Department
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Metallurgical Laboratory, Chemical Research - Radiation Chemistry, Report for the Period Ending January 15, 1945

Description: Technical report with short reports covering (1) Effect of radiation on water and aqueous systems; (2) Effect of neutrons on graphite; (3) Effect of radiation on solid compounds; and (4) Scattering, stopping-power, ion-pair production, etc.
Date: February 1, 1945
Creator: Burton, Milton, 1902- & Allen, A. O. (Augustine O.)
Partner: UNT Libraries Government Documents Department
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A Method of Recovering Thorium from Slag Materials

Description: Abstract. a method of recovering thorium from slag from the bomb process of producing thorium has been developed. HCl and NaOH are the only chemicals required in quantity. Materials required for a representative slag are given.
Date: March 23, 1945
Creator: Johnson, Oliver & Fisher, R. W.
Partner: UNT Libraries Government Documents Department
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Chemical Research -- Extraction and Properties of U233; Report for the Period Ending December 15, 1944

Description: Technical report containing short articles on (1) Determination of physical constants for U233; (2) Determination of decay chain of U233; (3) Extraction of U233; (4) Extracting solvents for uranium; (5) Factors affecting the extraction uranium and thorium by organic solvents, especially ether; and (6) Analysis of ore samples for protoactinium.
Date: February 24, 1945
Creator: Seaborg, Glenn T. (Glenn Theodore), 1912-1999; Manning, F. M. & Katzin, L. I.
Partner: UNT Libraries Government Documents Department
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Preliminary Report on a Colorimetric Method for the Determination of Microgram Quantities of Thorium : Experiments in the Dissolution of O2 Metal [UO2]

Description: Abstract. thorium can be precipitated as a salt of p-dimethylaminoazophenylarsonic acid at a pH of about 1.5. the precipitate, collected on a sintered glass filter is washed with dilute ammonium hydroxide to dissolve the dye. the amount of thorium is determined by measuring the concentration of the dye spectrophotometrically at a wavelength of 450 millimicrons. Zirconium, which interferes, can be separated and determined using the same reagent in strong hydrochloric. the behavior of thorium… more
Date: January 1, 1945
Creator: Byerly, W.; Niedrach, L.; Davin, W.; Dyas, H. & Bane, R. W.
Partner: UNT Libraries Government Documents Department
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Complexing Agents for the Solvent Extraction of Uranium from Thorium. I. The Use of Thiocyanate in the Extraction of Uranium. II. The Use of Antipyrine in Solvent Extraction

Description: Abstract. In the first section of this technical report a new method of extracting uranium from thorium nitrate solution is discussed. This method consists of extracting an aqueous solution of thorium nitrate, nitric acid, sodium sulphate, and potassium thiocyanate with hexone. By this procedure, using an equal volume of hexone it is possible to extract 83 percent of the uranium while only 0.3 percent of the thorium is extracted. other experiments show that even greater separations are possi… more
Date: February 16, 1945
Creator: Reas, W. H.
Partner: UNT Libraries Government Documents Department
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Metallurgical Laboratory, Chemical Research - Radiation Chemistry, Report for the Month Ending March 15, 1945

Description: Technical report with short reports on (1) Effect of radiation on water and aqueous systems; (2) Gas evolution from uranyl solutions; (3) Effect of radiation on solid compounds; (4) Instruments; and (5) Scattering.
Date: March 15, 1945
Creator: Burton, Milton, 1902- & Allen, A. O. (Augustine O.)
Partner: UNT Libraries Government Documents Department
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Analysis of Iron in Thorium, Beryllium, and Cerium

Description: Introduction. the colorimetric determination of iron based on the formation of the colored ferrous-1,10-phenanthroline complex has been used successfully by a number of investigators. In this technical report, its adaptation to the routine determination of iron in cerium, thorium, and beryllium metals and their compounds is described.
Date: September 10, 1945
Creator: Ericson, R. P & Fornefeld, E. J.
Partner: UNT Libraries Government Documents Department
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Extraction of Uranyl Nitrate and Thorium Nitrate by Organic Solvents

Description: Abstract. The separation of uranyl nitrate from aqueous solutions of 0.635 M thorium nitrate, 3 M nitric acid and 3 M calcium nitrate by extraction with organic solvents has been investigated. Solvents which gave good separations were 2-tthyl hexyl acetate, ethyl benzoate, n-butyl either and beta-beta- dichloroethyl ether. In general, higher esters, ethers and alcohols are better for separating uranium from thorium that the lower homologues. Several solvents were tested at lower nitric acid… more
Date: November 5, 1945
Creator: Johnson, O. & Newton, A. S.
Partner: UNT Libraries Government Documents Department
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Precipitation of Thorium Oxalate from Nitric Acid Solutions

Description: Introduction. It has been known for a long time that thorium is precipitated by oxalic acid in acid solutions, but a survey of the literature showed no study of the limits of the acidity and oxalic acid excess which yield quantitative results. V. I. Spitzin reports on the solubility of thorium oxalate in varying concentrations of several acids, but the effect of an excess oxalic acid is not included. Since solutions are sometimes presented for analysis that contain more than the recommended … more
Date: October 5, 1945
Creator: Ayers, A. S.
Partner: UNT Libraries Government Documents Department
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The Extraction of Uranium into Hexone as Uranyl Thiocyanate from Thorium Nitrate Solutions

Description: Technical report with six sections describing the process: (1) The reaction of HN)3 with HSCN; (2) The distribution of nitric acid between hexone and water; (3) The distribution of HSCN between hexone and water; (4) The solubility of thorium sulfate in various extraction solutions; (5) The distribution of protoactinium and fission elements between hexone and aqueous thiocyanate solutions; and (6) Separation of uranium from thorium by extraction into hexone as UO2(SCH)a.
Date: May 18, 1945
Creator: Reas, William H.
Partner: UNT Libraries Government Documents Department
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Sweeping of Fission Gases from Solutions of U and Plutonium

Description: Technical report describing two experiments performed to compare the amounts of fission gases swept out of UNH solution with those amounts swept out of PU solution under idential condiditons. The charge wire technique was used. The essential date and the results are given in tables in the report.
Date: September 4, 1945
Creator: Adams, R. M. & Finkelstein, H.
Partner: UNT Libraries Government Documents Department
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The Rapid Determination of Nitric Acid and Thorium in Thorium Nitrate Solutions

Description: Abstract. The physico-chemical methods of determining nitric acid and thorium nitrate in solutions containing these two materials were investigated. Conductimetric titration with sodium hydroxide can be used to determine nitric acid accurately. the titration of thorium nitrate requires a separate standardization of the base however, since a basic salt is precipitated rather the normal hydroxide. The titration of thorium is reproductible however, so and empirical standardization can be used.… more
Date: November 27, 1945
Creator: Newton, A. S.; Powell, J. (James), 1932- & Figard, P
Partner: UNT Libraries Government Documents Department
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Recovery of D2O and UO2F2 by Distillation

Description: Technical report describing the purification and separation by distillation of UO2F2 from D2O. In the experiment which is discussed 2,129.6 lbs of UO2F2 were dissolved in 6,605 lbs of D2O. The average isotopic purity of the D2O decreased during the distillation from 99.77% to 99.73%. The dissolved impurities were less than those present originally in the heavy water.
Date: October 10, 1945
Creator: Fischer, R. & Wattenberg, Albert, 1917-
Partner: UNT Libraries Government Documents Department
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A Study of Thorium Peroxide Sulfate

Description: Abstract. Thorium peroxide was precipitated from thorium nitrate solutions containing varying amounts of sulfate ion and of hydrogen ion. The washed solids were analyzed both wet and dry. Analyses were made for thorium, peroxide oxygen, sulfate, nitrate, and water contents. X-ray powder photographs of the dried samples by W.H. Zachariasen showed the presence of only two phases. When precipitated from high sulfuric acid, the solid phase was isomorphous with Th(OO)SO4.3H20. More weakly acid … more
Date: October 1, 1945
Creator: Hamaker, John W.
Partner: UNT Libraries Government Documents Department
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The Digging-in of a Warped Rod Into a Rib

Description: Abstract. Some rather idealized considerations are given regarding the depth a warped rod presses into the ribs at the places of contact. It appears that this distance may, under some conditions, be of the order of 70 times greater than for a straight rod resting uniformly on the ribs.
Date: January 22, 1945
Creator: Martin, A. V.
Partner: UNT Libraries Government Documents Department
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The Effect of Thermal Cycling on the Thermal Transfer from a Sand Blasted Slug to an Unbonded Jacket

Description: Abstract. Measurements were made to determine the effect of thermal cycling on heat transfer from slug to jack using a slug with a sand blasted surface. The value of the transfer coefficient h decreased from initial values ranging from 10 to [formula], to values and [formula] after 1700 cycles, and to a range of 0.15 to 0.45 [formula] after 3200 cycles. Comparisons are made with the results found for slugs with different surfaces.
Date: April 2, 1945
Creator: Bentley, Robert R.
Partner: UNT Libraries Government Documents Department
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The Hall Effect in Neutron Irradiated and Annealed Graphite

Description: Abstract. Irradiated Whiting graphite possesses a small negative or a positive Hall constant, depending upon the dosage. Annealing at 500 degrees C for 1 hour in helium results in a Hall constant which is large in magnitude and negative in sign. The properties of the annealed graphite are presumably close to those of the original unirradiated material. Unirradiated AGOT-K graphite has a large, negative Hall constant. A mechanism is suggested which accounts for the change in sign of the Hall con… more
Date: April 18, 1945
Creator: Maurer, Robert J. & Ruder, Richard C.
Partner: UNT Libraries Government Documents Department
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A Note on the Kinetics of Homogeneous Piles

Description: Abstract. In investigating stability of a homogeneous pile it has been customary to assume that the production of bubbles follows the production of power instantaneously. Here we investigate the implications of introduction of an intermediate dissolved gas stage under two hypotheses on the formation of bubbles from this dissolved gas. It is seen that this additional stage tends to make the pile unstable.
Date: June 26, 1945
Creator: Wilkins, J. Ernest, Jr., 1923-2011
Partner: UNT Libraries Government Documents Department
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The Production of Ceramic Ware by Slip-Casting

Description: This report discusses the production of ceramic ware through the process of slip-casting. The report separately describes the processes of creating zirconia ware, beryllia ware, alundum ware, thoria ware, and specially shaped ceramic ware.
Date: October 20, 1945
Creator: Calderwood, Wayne
Partner: UNT Libraries Government Documents Department
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Note: Positive Ion Gun for the Notre Dame Van de Graaff-Herb Generator

Description: "This report is based on work done at the University of Notre Dame under the auspice of the Manhattan District under contract No. W-7405-Eng-49." This report discusses the operation and purpose of the positive ion gun for the Notre Dame's Van de Graaf-herb generator
Date: 1945
Creator: Wiedenbeck, M. L.
Partner: UNT Libraries Government Documents Department
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Studies of Porphyrin Metabolism, 3. The Relation of Erythropoiesis to the Excretion of Coproporphyrin by Dogs and Rabbits, and to the Concentration of Coproporphyrin and Protoporphyrin in Rabbit Erythrocytes

Description: Report discussing studies regarding porphyrin excretion and hemoglobin metabolism in animals with phenylhydrazine anemia, and studies regarding the coproporphyrin and protoporphyrin in the red blood cells of rabbits.
Date: November 25, 1945
Creator: Schwartz, Samuel; Glickman, Marcia; Hunter, Rosie & Wallace, Jean
Partner: UNT Libraries Government Documents Department
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