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Recovery of Tuballoy (Uranium) From Tantalum

Description: Report discussing methods for the "separation of tantalum and tuballoy from used tantalum K's. These methods are: hydrofluorination, fluorination, hydrochlorination and dissolution in hydrofluoric acid -- nitric acid, hydrofluoric acid -- hydrochloric acid mixture, and hydrofluoric acid alone."
Date: September 29, 1945
Creator: Johnston, C. P. & Milch, A.
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Recovery of uranium and plutonium from Redox off-standard aqueous waste streams

Description: In the operation of countercurrent extraction columns as in the Redox process, it is possible, and probable, that from unexpected behaviour of a column, operator error, colloid formation, etc., there will result from time to time excessive losses of uranium and plutonium in the overall process. These losses will naturally accumulate in the waste streams, particularly in the aqueous waste streams. If the loss is excessively high, and such lost material can be recovered by some additional method,… more
Date: December 31, 1949
Creator: Holm, C. H. & Matheson, A. R.
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Recovery of Uranium From Beta Salvage Residues by Vapor Phase Chlorination With CCl₄

Description: Abstract: A simple process to recover the bulk of the uranium from ignited beta salvage residues was sought. In preliminary experiments a vapor phase chlorination with CCl₄ for about four hours followed by water and nitric acid leaching was found adequate. Recoveries are estimated at 60 to 90% of the total uranium content.
Date: April 22, 1946
Creator: Veatch, R. W., Jr. & Miller, A. J.
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Recovery of Uranium From Contaminated Precipitron Oil

Description: Abstract: The distillation and residue extraction recovery procedures developed for the recovery of uranium from Kinney and diffusion pump oil, were applied to contaminated precipitron oil. The effectiveness and advisability of using the method, in whole or in part, is discussed, and various recommendations for processing this particular type of oil are presented. Additional contaminating substances present in this type of oil added to the complexity of the problem but a satisfactory recovery p… more
Date: April 17, 1947
Creator: Lee, J. E.; Aikin, L. M. & Susano, C. D.
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Recovery of Uranium From Fiberglass Air Filters

Description: Abstract: Various procedures for extracting uranium from fiberglass air filters have been tested and compared. Satisfactory results which involve the least amount of handling are obtained by simply washing the material with hot 1:1 hydrochloric acid.
Date: August 5, 1946
Creator: Adams, R. H.; Rogers, J. A. & Brown, K. B.
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Recovery of Uranium From Oil Distillation Residue

Description: Abstract: The complete development of an effective process for recovery of the uranium in the residues from distillation of used Kinney and diffusion pump oils or similar oils is described. After considerable study and experimentation with several methods, a successful procedure has been developed. The recommended procedure embodies solution of the residues in trichlorethylene followed by extraction with nitric acid. Recovery of uranium is better than 99 percent effective and the method may be … more
Date: February 24, 1947
Creator: Lee, J. E.; Aikin, L. M. & Susano, C. D.
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Rectangular Shell Plating Under Uniformly Distributed Hydrostatic Pressure

Description: "A check of the calculation methods used by Foppl and Henky for investigating the reliability of shell plating under hydrostatic pressure has proved that the formulas yield practical results within the elastic range of the material. Foppl's approximate calculation leaves one on the safe side. It further was found on the basis of the marked ductility of the shell plating under tensile stress that the strength is from 50 to 100 percent higher in the elastic range than expected by either method" (… more
Date: December 1940
Creator: Neubert, M. & Sommer, A.
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Redox Committee: Conference notes and recommendations, April 5, 1949

Description: The notes and recommendations contained in this report relate to the design and construction of the Redox Production Plant with its associated Tank Farm at Hanford. All current development work for the Redox Program was to be transferred to the Redox Production Plant. [The Redox plant used a reduction-oxidation process for fuel separation that allowed recovery of uranium as well as plutonium for the first time. It succeeded earlier plants (T and B) that used methods based on the bismuth phospha… more
Date: April 5, 1949
Creator: Greager, O. H.; MacCready, W. K. & Seckendorff, E. W.
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Redox Committee: Conference notes and recommendations, meeting of April 11, 1949

Description: This report discusses recommendations for development work on the Redox Production Plant. It contains an outline for a relationship procedure between the architect engineer and General Electric Design Division; preparation of a material balance and process flow; the preparation of engineering flow diagrams, including lists of standard symbols for these diagrams; a material and equipment list; a project cost estimate; and Procedures covering institution and execution of work involving studies by… more
Date: April 11, 1949
Creator: Greager, O. H.; MacCready, W. K. & Seckendorff, E. W.
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Redox Committee: Conference notes and recommendations, meeting of June 9, 1949

Description: The report includes recommendations on flow sketches; 68% nitric acid specifications; dissolver off-gas and ventilation air treatment; installation of standby equipment (details included in Appendix A); schedule of scope drawing specifications and arrangement drawings; mechanical development program (details included in Appendix B); and scope of work on waste disposal facilities (Appendix C).
Date: June 9, 1949
Creator: Greager, O. H.; MacCready, W. K. & Seckendorff, E. W.
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Redox Committee: Conference notes and recommendations, meeting of June 13, 1949

Description: Recommendations discussed included the transfer of Waste Metal Recovery from the Kellex Corporation; the Kellex contract revisions for their work on the design of the Redox Production Plant; procurement and inspection procedures; aluminum nitrate supply and procurement; and waste recovery with the tributyl phosphate and hexane process.
Date: June 14, 1949
Creator: Greager, O. H.; MacCready, W. K. & Seckendorff, E. W.
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Redox Committee: Conference notes and recommendations, meeting of June 16, 1949

Description: Topics discussed included scope of work by the Kellex Corporation; Redox Production Plant procurement; bearing capacity of soils and other site characterization for the Redox Production Plant site; purchase of Moyno pumps; scope drawing schedules; 68% nitric acid requirements for the process; pump development for the Redox Production Plant; vessel specifications; Design basis letters on electrical distribution, steam distribution, raw and filtered water distribution, and railroads. The report i… more
Date: June 20, 1949
Creator: Greager, O. H.; MacCready, W. K. & Seckendorff, E. W.
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Redox Committee: Conference notes and recommendations, meeting of June 23, 1949

Description: Topics discussed include gang valve substitute devices; cost of lining cell bottom with stainless steel; and the pump development program. [The Redox plant used a reduction-oxidation process for fuel separation that allowed recovery of uranium as well as plutonium for the first time. It succeeded earlier plants (T and B) that had used methods based on the bismuth phosphate process that recovered only plutonium.]
Date: June 23, 1949
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Redox Committee: Conference notes, meeting of May 23, 1949

Description: Discussions included the aluminum nitrate recovery process; specifications for process pumps; a review of the safety of the Redox process; plans for the proposed Waste Tank Farm, retention basin, diversion box, and cribs; and a request from the US AEC for a concise summary of the entire Redox program.
Date: May 23, 1949
Creator: Greager, O. H.; MacCready, W. K. & Seckendorff, E. W.
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