Date: October 31, 2004
Creator: (UTK), Jay Frankel & (UTK), Adrian Sabau
Description: One of the main barriers in the analysis and design of materials processing and industrial applications is the lack of accurate experimental data on the thermophysical properties of materials. To date, the measurement of most of these high-temperature thermophysical properties has often been plagued by temperature lags that are inherent in measurement techniques. These lags can be accounted for with the appropriate mathematical models, reflecting the experimental apparatus and sample region, in order to deduce the desired measurement as a function of true sample temperature. Differential scanning calorimeter (DSC) measurements are routinely used to determine enthalpies of phase change, phase transition temperatures, glass transition temperatures, and heat capacities. In the aluminum, steel, and metal casting industries, predicting the formation of defects such as shrinkage voids, microporosity, and macrosegregation is limited by the data available on fraction solid and density evolution during solidification. Dilatometer measurements are routinely used to determine the density of a sample at various temperatures. An accurate determination of the thermophysical properties of materials is needed to achieve accuracy in the numerical simulations used to improve or design new material processes. In most of the instruments used to measure properties, the temperature is changed according to instrument controllers ...
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