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DEVELOPMENT OF CONTINUOUS SOLVENT EXTRACTION PROCESSES FOR COAL DERIVED CARBON PRODUCTS

DEVELOPMENT OF CONTINUOUS SOLVENT EXTRACTION PROCESSES FOR COAL DERIVED CARBON PRODUCTS

Date: December 31, 2009
Creator: Kennel, Elliot; Chen, Chong; Dadyburjor, Dady; Heavner, Mark; Katakdaunde, Manoj; Magean, Liviu et al.
Description: This NETL sponsored effort seeks to develop continuous technologies for the production of carbon products, which may be thought of as the heavier products currently produced from refining of crude petroleum and coal tars obtained from metallurgical grade coke ovens. This effort took binder grade pitch, produced from liquefaction of West Virginia bituminous grade coal, all the way to commercial demonstration in a state of the art arc furnace. Other products, such as crude oil, anode grade coke and metallurgical grade coke were demonstrated successfully at the bench scale. The technology developed herein diverged from the previous state of the art in direct liquefaction (also referred to as the Bergius process), in two major respects. First, direct liquefaction was accomplished with less than a percent of hydrogen per unit mass of product, or about 3 pound per barrel or less. By contrast, other variants of the Bergius process require the use of 15 pounds or more of hydrogen per barrel, resulting in an inherent materials cost. Second, the conventional Bergius process requires high pressure, in the range of 1500 psig to 3000 psig. The WVU process variant has been carried out at pressures below 400 psig, a significant difference. Thanks ...
Contributing Partner: UNT Libraries Government Documents Department
Shear Strength Measurement Benchmarking Tests for K Basin Sludge Simulants

Shear Strength Measurement Benchmarking Tests for K Basin Sludge Simulants

Date: June 10, 2009
Creator: Burns, Carolyn A.; Daniel, Richard C.; Enderlin, Carl W.; Luna, Maria & Schmidt, Andrew J.
Description: Equipment development and demonstration testing for sludge retrieval is being conducted by the K Basin Sludge Treatment Project (STP) at the MASF (Maintenance and Storage Facility) using sludge simulants. In testing performed at the Pacific Northwest National Laboratory (under contract with the CH2M Hill Plateau Remediation Company), the performance of the Geovane instrument was successfully benchmarked against the M5 Haake rheometer using a series of simulants with shear strengths (τ) ranging from about 700 to 22,000 Pa (shaft corrected). Operating steps for obtaining consistent shear strength measurements with the Geovane instrument during the benchmark testing were refined and documented.
Contributing Partner: UNT Libraries Government Documents Department
The Muon LINAC for the International Design Study of the Neutrino Factory

The Muon LINAC for the International Design Study of the Neutrino Factory

Date: September 1, 2011
Creator: A. Kurup, C. Bontoiu, Morteza Aslaninejad, J. Pozimski, A. Bogacz, V.S. Morozov, Y.R. Roblin, K.B. Beard
Description: The first stage of muon acceleration in the Neutrino Factory utilises a superconducting linac to accelerate muons from 244 MeV to 900 MeV. The linac was split into three types of cryomodules with decreasing magnetic fields and increasing amounts of RF voltage but with the design of the superconducting solenoid and RF cavities being the same for all cryomodules. The current status of the muon linac for the International Design Study for the Neutrino Factory will be presented including a final lattice design of the linac and tracking simulations.
Contributing Partner: UNT Libraries Government Documents Department
Building Energy Audit Report for Pearl Harbor, HI

Building Energy Audit Report for Pearl Harbor, HI

Date: September 30, 2010
Creator: Brown, Daryl R.; Chvala, William D.; De La Rosa, Marcus I. & Dixon, Douglas R.
Description: A building energy audit was performed by a team of engineers from Pacific Northwest National Laboratory (PNNL) under contract to the Department of Energy/Federal Energy Management Program (FEMP). The effort used the Facility Energy Decision System (FEDS) model to determine how energy is consumed at selected Pearl Harbor buildings, identify cost-effective energy retrofit measures, and calculate the potential energy and cost savings. This report documents the findings of that assessment.
Contributing Partner: UNT Libraries Government Documents Department
Complexation of NpO2+ with N-methyl-iminodiacetic Acid: in Comparison with Iminodiacetic and Dipicolinic Acids

Complexation of NpO2+ with N-methyl-iminodiacetic Acid: in Comparison with Iminodiacetic and Dipicolinic Acids

Date: October 1, 2010
Creator: Tian, Guoxin & Rao, Linfeng
Description: Complexation of Np(V) with N-methyl-iminodiacetic acid (MIDA) in 1 M NaClO{sub 4} solution was studied with multiple techniques including potentiometry, spectrophotometry, and microcalorimetry. The 1:2 complex, NpO{sub 2}(MIDA){sub 2}{sup 3-} was identified for the first time in aqueous solution. The correlation between its optical absorption properties and symmetry was discussed, in comparison with Np(V) complexes with two structurally related nitrilo-dicarboxylic acids, iminodiacetic acid (IDA) and dipicolinic acid (DPA). The order of the binding strength (DPA > MIDA > IDA) is explained by the difference in the structural and electronic properties of the ligands. In general, the nitrilo-dicarboxylates form stronger complexes with Np(V) than oxy-dicarboxylates due to a much more favorable enthalpy of complexation.
Contributing Partner: UNT Libraries Government Documents Department
Small Reactor Designs Suitable for Direct Nuclear Thermal Propulsion: Interim Report

Small Reactor Designs Suitable for Direct Nuclear Thermal Propulsion: Interim Report

Date: January 1, 2012
Creator: Schnitzler, Bruce G.
Description: Advancement of U.S. scientific, security, and economic interests requires high performance propulsion systems to support missions beyond low Earth orbit. A robust space exploration program will include robotic outer planet and crewed missions to a variety of destinations including the moon, near Earth objects, and eventually Mars. Past studies, in particular those in support of both the Strategic Defense Initiative (SDI) and the Space Exploration Initiative (SEI), have shown nuclear thermal propulsion systems provide superior performance for high mass high propulsive delta-V missions. In NASA's recent Mars Design Reference Architecture (DRA) 5.0 study, nuclear thermal propulsion (NTP) was again selected over chemical propulsion as the preferred in-space transportation system option for the human exploration of Mars because of its high thrust and high specific impulse ({approx}900 s) capability, increased tolerance to payload mass growth and architecture changes, and lower total initial mass in low Earth orbit. The recently announced national space policy2 supports the development and use of space nuclear power systems where such systems safely enable or significantly enhance space exploration or operational capabilities. An extensive nuclear thermal rocket technology development effort was conducted under the Rover/NERVA, GE-710 and ANL nuclear rocket programs (1955-1973). Both graphite and refractory metal ...
Contributing Partner: UNT Libraries Government Documents Department
PREDICTION OF DISSOLVER LIFETIMES THROUGH NON-DESTRUCTIVE EVALUATION AND LABORATORY TESTING

PREDICTION OF DISSOLVER LIFETIMES THROUGH NON-DESTRUCTIVE EVALUATION AND LABORATORY TESTING

Date: October 3, 2011
Creator: Mickalonis, J.; Woodsmall, T.; Hinz, W. & Edwards, T.
Description: Non-destructive evaluation was used as the primary method of monitoring the corrosion degradation of nuclear material dissolvers and assessing the remaining lifetimes. Materials were typically processed in nitric acid based (4-14M) solutions containing fluoride concentrations less than 0.2 M. The primary corrosion issue for the stainless steel dissolvers is the occurrence of localized corrosion near the tank bottom and the heat affected zones of the welds. Laboratory data for a range of operational conditions, including solution chemistry and temperature, was used to assess the impact of processing changes on the dissolver corrosion rate. Experimental and NDE-based general corrosion rates were found to be in reasonable agreement for standard dissolution chemistries consisting of nitric acid with fluorides and at temperatures less than 95 C. Greater differences were observed when chloride was present as an impurity and temperatures exceeded 100 C.
Contributing Partner: UNT Libraries Government Documents Department
New Superheavy Element Isotopes: 242Pu(48Ca,5n)285114

New Superheavy Element Isotopes: 242Pu(48Ca,5n)285114

Date: October 22, 2010
Creator: Ellison, Paul A; Gregorich, Kenneth E.; Berryman, Jill S.; Bleuel, Darren L.; Clark, Roderick M.; Dragojevic, Irena et al.
Description: The new, neutron-deficient, superheavy element isotope {sup 285}114 was produced in {sup 48}Ca irradiations of {sup 242}Pu targets at a center-of-target beam energy of 256 MeV (E* = 50 MeV). The {alpha} decay of {sup 285}114 was followed by the sequential {alpha} decay of four daughter nuclides, {sup 281}Cn, {sup 277}Ds, {sup 273}Hs, and {sup 269}Sg. {sup 265}Rf was observed to decay by spontaneous fission. The measured {alpha}-decay Q values were compared with those from a macroscopic-microscopic nuclear mass model to give insight into superheavy element shell effects. The {sup 242}Pu({sup 48}Ca,5n){sup 285}114 cross section was 0.6{sub -0.5}{sup +0.9} pb.
Contributing Partner: UNT Libraries Government Documents Department
Analysis of Possible Stratagems for Enhancing the EOM Power of RTGs for the CRAF Mission

Analysis of Possible Stratagems for Enhancing the EOM Power of RTGs for the CRAF Mission

Date: August 1, 1991
Creator: Schock, Alfred; Or, Chuen T & Noravian, Heros
Description: Paper presented at the 26th IECEC in Boston, MA August 4-9, 1991. This paper describes the various stratagems investigated and discusses their drawbacks and their effectiveness. The analytical results indicated that a combination of relatively modest RTG modifications that could be implemented in time for the mission could come very close to meeting the CRAF power demand goals specified by JPL. However, since even with the modifications the two RTGs did not provide sufficient margin for possible further growth in power demand, the JPL project team ultimately decided to use 3 RTGs for the CRAF mission also. This had the decisive advantage of eliminating the need for load switching to reduce the power demand peaks. The purpose of this paper is to document the various power enhancement schemes analyzed and their computed effectiveness, for possible future applications. There are three copies in the file.
Contributing Partner: UNT Libraries Government Documents Department
A new concept of vertically integrated pattern recognition associative memory

A new concept of vertically integrated pattern recognition associative memory

Date: November 1, 2011
Creator: Liu, Ted; Hoff, Jim; Deptuch, Grzegorz; Yarema, Ray & /Fermilab
Description: Hardware-based pattern recognition for fast triggering on particle tracks has been successfully used in high-energy physics experiments for some time. The CDF Silicon Vertex Trigger (SVT) at the Fermilab Tevatron is an excellent example. The method used there, developed in the 1990's, is based on algorithms that use a massively parallel associative memory architecture to identify patterns efficiently at high speed. However, due to much higher occupancy and event rates at the LHC, and the fact that the LHC detectors have a much larger number of channels in their tracking detectors, there is an enormous challenge in implementing fast pattern recognition for a track trigger, requiring about three orders of magnitude more associative memory patterns than what was used in the original CDF SVT. Scaling of current technologies is unlikely to satisfy the scientific needs of the future, and investments in transformational new technologies need to be made. In this paper, we will discuss a new concept of using the emerging 3D vertical integration technology to significantly advance the state-of-the-art for fast pattern recognition within and outside HEP. A generic R and D proposal based on this new concept, with a few institutions involved, has recently been submitted to DOE ...
Contributing Partner: UNT Libraries Government Documents Department