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Fabrication of Uranium Wire

Description: From abstract: "The present report describes experimental work performed to establish a procedure for the production of uranium metal wire. In all cases, the size of the initial rod was 1/2 inch diameter. Three materials were used: hot extruded tuballoy rod, high purity cast tuballoy rod, and cast U-235 rod."
Date: October 25, 1949
Creator: Anderson, R. E.; Taub, J. M. & Doll, D. T.
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Spontaneous Fission of 48

Description: Report discussing an experiment to reinvestigate the spontaneous fission of 48 (Pu-238) in an effort to determine a more accurate value for the spontaneous fission constant that was found in a previous experiment.
Date: December 19, 1949
Creator: Jungerman, John A.
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A Microdetermination of Uranium by Ferric Sulfate Titration

Description: Abstract: "Following nitrate removal by means of a three-stage hydrochloric acid digestion, uranium was reduced with chromous sulfate reagent. In an inert atmosphere, the quadrivalent uranium was titrated at 80-95[degrees] with standard ferric sulfate solution. The end point was obtained with a potentiometric cell including a platinum in-titrant reference electrode and a platinum indicator electrode. Application was made to various low leverl uranium solutions. For samples containing 1 - 12 mil… more
Date: February 16, 1949
Creator: Christopherson, E. W.
open access

Corrosion Tests on Tantalum, Hastelloy C and Duriron in 234-5 Project Solutions

Description: Introduction: "Room temperature and elevated temperature, static immersion and vapor suspicion, corrosion tests were conducted with Duriron, Hastelloy C, and tantalum in hydriotic acid and 234-5 project process supernatant solution (synthetic environments. The data relevant to these tests are contained herein."
Date: February 25, 1949
Creator: Work, J. B. & Koenig, W. W.
open access

Optical Instruments for the Atomic Industry

Description: The following report presents some points of interest obtained from the use of optical equipment at the Hanford Works; however, this report does not give complete descriptions of the instruments or theories. Full descriptions can be found in the Instrument Division Manual, Section IV.
Date: 1949
Creator: Holeman, J. M.
open access

The Critical Mass of a Spherical Reactor with Variable Intrinsic Buckling

Description: Abstract: "The critical mass both of an untamped and water-tamped sphere with parabolic radial variation of the intrinsic buckling is calculated by a perturbation method. The result is applied to finding the minimum critical mass of plutonium in water suspension with infinite water temper; the calculations show that the minimum critical mass at constant concentration may be reduced by an amount of the order of 7.6% when the concentration of plutonium is permitted to vary throughout the suspensi… more
Date: April 28, 1949
Creator: Muller, G. M.
open access

Determination of Organic Acids in Process Solutions

Description: Abstract: "A method has been established for the estimation of volatile organic acids in aqueous process solutions containing UNH, nitric acid, ANN, sodium dichromate and small amounts of hexone. The practice is to distill a 400 ul or 500 ul sample in the presence of an excess of phosphoric acid and ferrous sulfate under a high vacuum; a special apparatus utilizing a receiver cooled with a dry ice-isopropanol mixture is employed. The distillate is taken up in isopropanol and then titrated poten… more
Date: June 29, 1949
Creator: Brouns, R. J. & Pollock, C. W.
open access

The Coulometric Titration of 8-Hydroxyquinoline

Description: Abstract: "A new method of determining 8-hydroxyquinoline by titration with electrolytucally-generated bromine has been developed. Results show good precision in the range 0.4 mg. to 1.6 mg. total 8-hydroxyquinoline, with 99% confidence limits of less than +/- 2%. An electronically-regulated constant current source, required by the method, is described. A new indicator system with high sensitivity to free bromine is discussed."
Date: June 16, 1949
Creator: Carson, W. N.
open access

The Coulometric Determination of Acetic Acid

Description: Abstract: "Small amounts of acetic acid, equivalent to 400 ul. of 0.3 to 0.13 g/L. can be titrated coulonatrically in the presence of a 10 to 25-fold excess of HN03 in 70%, isopropanol. An accuracy of +/- 0.1% and a precision of +/- 8.5% (99% limite) are obtained.
Date: August 16, 1949
Creator: Carson, W. N. & Ko, Roy
open access

The Spectrochemical Analysis of Hafnium and Zirconium

Description: Abstract: "The analysis of hafnium and zirconium by the copper spark technique is presented for solutions of HCl, HF, and HClO4 acids. The special techniques of electrode protection and vacuum drying of perchloric acid samples are outlined. Also given are the working curves and deviations of both elements."
Date: March 16, 1949
Creator: Conway, John G. & Moore, Milton F.
open access

The Preparation and Properties of Uranium Trifluoride

Description: From abstract: "The means of preparing uranium trifluoride are discussed. The most practical method is the reduction of uranium tetrafluoride with uranium although reduction with hydrogen or atomic hydrogen may also be feasible...A literature survey and discussion of other means of preparation are given."
Date: 1949
Creator: Warf, James C.
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