UNT Libraries Government Documents Department - 122 Matching Results

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Abrasive Blasting for Cleaning Parts

Description: Abstract: A demonstration on August 22, 1945, showed that Alpha or Beta M or K parts, including insulators, can be well cleaned with a pressure-feed abrasive blaster. The abrasive is a slurry of alumina and water mixed with high velocity air in a special feed nozzle. The slurry is continuously recycled.
Date: September 1945
Creator: McWherter, Jack R. & Yerazunis, Stephen
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Analysis for Oxide in Thorium Metal

Description: Abstract. to estimate the oxygen picked up by thorium in casting a rapid method of running the acid insoluble content was developed. the quickest procedure consists of reacting with mixed acids, fuming with perchloric and filtration to separate the "free" thorium from the "combined". The precipitate is ignited and weighed as thorium dioxide.
Date: May 12, 1945
Creator: Ayers, A. S.
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Analysis of Heavy Water by Equilibration

Description: Technical report discussing that the deuterium concentration of heavy water can be determined by equilibrating the water with deuterium gas in the presence of a catalyst with subsequent analysis of the equilibrated gas on the mas spectrometer. The apparatus for equilibration analyses maybe be considered in three parts: 1) apparatus for introducing the ingredients into the reaction chambers; 2) the reaction chambers; 3) the mass spectrometer for analysis of the equilibrated gas. The isotopic co… more
Date: May 15, 1945
Creator: Fischer, R. B.; Potter, R. A. & Voskuyl, R. J.
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Analysis of Iron in Thorium, Beryllium, and Cerium

Description: Introduction. the colorimetric determination of iron based on the formation of the colored ferrous-1,10-phenanthroline complex has been used successfully by a number of investigators. In this technical report, its adaptation to the routine determination of iron in cerium, thorium, and beryllium metals and their compounds is described.
Date: September 10, 1945
Creator: Ericson, R. P & Fornefeld, E. J.
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Analysis of TH( NO3 ) -Ca( NO3 )2 –HNO3 Solutions

Description: Abstract. Methods of analysis for thorium, calcium, and nitric acid in solutions from thorium extraction purification columns are described and the results and errors are outlined. A brief description of methods of analysis that were not successful is included.
Date: December 20, 1945
Creator: Warf, James C.; Patterson, J. H. & Banks, Charles V.
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Analysis of Uranium-Manganese Alloys

Description: Introduction. the conventional procedures of analysis for uranium and manganese can be employed in the analysis of alloys of these metals. The alloys are reacted with perchloric acid and hydrogen peroxide, fumed to remove any chloride ions, diluted to volume and aliquots analyzed by redoximetry.
Date: October 5, 1945
Creator: Ayers, A. S.
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Analysis of Uranium-Nicked Alloys

Description: Abstract. Methods for determination of both uranium and nickel in solutions of these metals are described. Alloys can be dissolved in nitric acid treated with citric acid to complex the uranium, and the nickel precipitated as nicked dimethylglyoxime. The uranium is reduced and titrated with standard ceric sulfate. These methods are for the determination of macro amounts of uranium and nickel with errors on the order of 0.1%.
Date: June 7, 1945
Creator: Ericson, R. P.
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Application of Conductivity Measurements to a Study of (a) Complex Formation Between F[ Gamma] + and F- and Al+ + + and F- (b) Titration of F- Ion with H + Ion

Description: From introduction: This report describes some preliminary electro-conductometric titrations which were made in order to ascertain whether the method [for selecting the best complexing agent for any problem that may arise] gave interpretable results.
Date: 1945
Creator: Tober, Frank W., 1919-1995 & Larson, Clarence E.
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Chemical Research -- Extraction and Properties of U233; Report for the Period Ending December 15, 1944

Description: Technical report containing short articles on (1) Determination of physical constants for U233; (2) Determination of decay chain of U233; (3) Extraction of U233; (4) Extracting solvents for uranium; (5) Factors affecting the extraction uranium and thorium by organic solvents, especially ether; and (6) Analysis of ore samples for protoactinium.
Date: February 24, 1945
Creator: Seaborg, Glenn T. (Glenn Theodore), 1912-1999; Manning, F. M. & Katzin, L. I.
open access

The Chlorination of TO₃

Description: Abstract: The applicability of specific mixtures and organic chlorocarbons in general toward the chlorination of TO₃ has been tested by means of reactions is sealed glass tubes. The results show that thionyl chloride mixed with tetrachloroethylene or a bromothane of the tyoe CHBrC12 will produce TCI4 directly. This same result is produced by CBr2C12 alone.
Date: December 28, 1945
Creator: Gavlin, Gilbert; Hubbard, J. V. & Clewett, G. H.
open access

Cleaning E-Units by Blasting

Description: Abstract: An air-water-abrasive blasting system thoroughly cleans copper parts of E units without damage to the parts. Little abrasive is required because of the continuous recycle of the abrasive slurry.
Date: 1945
Creator: McWherter, Jack R. & Yerazunis, Stephen
open access

Clinton Engineer Works Division of Chemical Research and Development Monthly Report: May/June 1945

Description: A report about the ongoing work regarding density. Attention was directed toward the accurate ascertainment of the T losses involved in a process in which the partially dried peroxide is transferred from the sintered glass funnels to the gold boats, and in which the calcination is male from TO4 to T3OE under nitrogen in the green salt reactors.
Date: 1945
Creator: Tennessee Eastman Corporation. Clinton Engineer Works. Division of Chemical Research and Development.
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Colorimetric Analysis for Cadmium - Diphenylthiocarbazone (Dithizone) Method

Description: Abstract: The well known colorimetric method for determining cadmium by means of dithizone has been reinvestigated and found applicable to solutions containing interfering ions much as are found in the plant. Copper, however, must be removed prior to using this analytical procedure.
Date: 1945
Creator: Schaap, W. B.; Farber, H.; Andrews, L. J. & Gates, J. W., Jr.
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Complexing Agents for the Solvent Extraction of Uranium from Thorium. I. The Use of Thiocyanate in the Extraction of Uranium. II. The Use of Antipyrine in Solvent Extraction

Description: Abstract. In the first section of this technical report a new method of extracting uranium from thorium nitrate solution is discussed. This method consists of extracting an aqueous solution of thorium nitrate, nitric acid, sodium sulphate, and potassium thiocyanate with hexone. By this procedure, using an equal volume of hexone it is possible to extract 83 percent of the uranium while only 0.3 percent of the thorium is extracted. other experiments show that even greater separations are possi… more
Date: February 16, 1945
Creator: Reas, W. H.
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Composition and Thermal Decomposition of Uranyl Peroxide

Description: Technical report on the studies that have been made on the composition and thermal decomposition of uranyl peroxide. The conditions of precipitation and drying have been found to have no appreciable effect on the composition of the compound, but do affect the physical appearance of the precipitate and the rate of thermal decomposition. The UO4 + 2H2O appears to be thermodynamically unstable with respect to UO3 at 25 degrees C and atmospheric pressure, although the rate of conversion is extreme… more
Date: June 30, 1945
Creator: Leininger, R. F.; Hunt, J. P. & Koshland, D. E., Jr.
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Crystal Structures of Some Uranium Compounds : a Summary from the Ames Laboratory

Description: Introduction. Some forty different uranium compounds have now been given diffraction study at Ames. Reports of these investigations are scattered in the Project literature; many have been reported in a sentence or two as a note along with chemical or metallographic reports. To make the results of this crystal structure work more available this summary of the Ames work has been compiled. (A similar summary has already been published from the Chicago laboratory.)
Date: August 15, 1945
Creator: Rundle, R. E.; Baenziger, N. C. & Wilson, A. S.
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The Determination of T at the Dropping Mercury Electrode in Hex Plant Ammonia and Peroxide Decantrates

Description: Inroduction: "A study of the literature, particularly the work done by R. Strubl, I.W. Kolthoff and S.B. Smith, indicated that a polargraphic method for the estimation of T could be devised which would not sacrifice reasonable accuracy for rapidity. Work was begun with the intention of developing such a method."
Date: January 16, 1945
Creator: Kwiatkowski, S.; Owens, J. & Casto, C. C.
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