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General Flattening and Power Curves

Description: Introduction: "In the evaluation of pile designs it is necessary to know how the production varies with the number of tubes. It has been possible to solve the problem in terms of some general parameters whose values may be quickly computed for any specific design when the pertinent information is available."
Date: March 30, 1953
Creator: Gast, Paul F.
open access

Ground Level Concentrations in the Vicinity of a 185 ft Stack

Description: Field tests were conducted to measure short-period pollutant concentrations at several stack heights during conditions of marked atmospheric instability and low wind speeds. The source was a mechanical smoke generator located at the 185-ft level of a tower.
Date: April 20, 1953
Creator: Shorr, B.
open access

Hanford Works Analytical Manual for Reactor Process Water

Description: Purpose: "The Hanford Works Analytical Manual for Process Water is designed to specify the analytical methods to be applied for control purposes in the Reactor Section, Process Sub-Section laboratories. The procedures are in general form and serve as references rather than outlined laboratory instructions. The manual us designed to replace the "Hanford Works Manual," HW-12862."
Date: February 13, 1953
Creator: Hanford Works
open access

A Hanford Works Vacuum System

Description: The remodeling, fabrication, and instrumentation of a high vacuum system are described. The faults encountered with the old system and their solution are outlined. Tests were made on diffusion pump oils and on the reduction of pump oil back diffusion. The measurement of high vacuum pressures by a cold cathode ionization gage at various points on a vacuum system are discussed.
Date: May 28, 1953
Creator: Holdreth, N. T.
open access

The Hydrogen Content of Fabricated Uranium

Description: The hydrogen contents of several types of fabricated uranium have been determined by a vacuum method and expressed in terms of ccH2/ccU. The data indicate that alpha-rolled metal contains about 0.25 ccH2(STP)/ccU whereas beta heat-treated uranium yielded values between 0.30 and 0.37 cc per cc. Restricted efforts were made to determine where in the heat treatment the 5 to 10 cc of hydrogen per slug were taken up. It appears that no one operation is wholly responsible for this additional gas, … more
Date: November 30, 1953
Creator: Ray, W. E. & Bowen, H. C.
open access

The Identification of the Angular Inclusions Present in Rolled Uranium

Description: Hanford uranium contains minute angular inclusions which affect the microstructure, reactivity, and other important factors controlling the serviceability of the metal. Small quantities of the inclusions have been isolated by chemical means, and the x-ray diffraction patterns and chemical analyses of the isolated materials have been determined. As a first step in the identification of the inclusions present in rolled uranium, a search was made for a chemical method of separating the inclusion… more
Date: May 15, 1953
Creator: Scott, F. A.
open access

The Identification of the Microscopic Angular Inclusions in Uranium

Description: Many procedures for the chemical isolation of the microscopic angular inclusions in rolled uranium have been investigated. Four were selected as most satisfactory for this work and will be described in detail. The procedures are: (1) the copper displacement of the uranium, (2) the electrolytic displacement of the uranium, (3) the chemical dissolution of the uranium in an anhydrous solution of hydrogen chloride in methanol, and (4) the chemical dissolution of the uranium in an aqueous solution… more
Date: December 14, 1953
Creator: Scott, F. A.
open access

In-Line Scintillation Gamma Monitor : Preliminary Specifications

Description: From introduction: "The following recommendations represent the best estimate, based on present knowledge, of the requirements for generally applicable or "universal" instrument for the continuous monitoring of radioactive process streams in terms of their gamma activity."
Date: January 22, 1953
Creator: Upson, U. L. & Connally, R. E.
open access

Investigation of Explosive Characteristics of Purex Solvent Decomposition Products (Red Oil)

Description: Abstract: "Laboratory production of an explosion between UNH and "red oil" under calcination conditions has been accomplished. Attempted production of a vapor phase explosion was unsuccessful below 150-160 C. Since such severe conditions are necessary to obtain an explosive reaction, it appears that present Purex plant design is adequate to avoid explosive conditions."
Date: March 17, 1953
Creator: Wagner, Robert M.
open access

An Ionization Chamber Method for the Standardization of Tritiated Water Samples

Description: Ionization measurements of water vapor in vapor-liquid equilibrium were made with a series of chambers on a tritiated water sample which was prepared by burning T2 to T2O and diluting it with H2O. A correction was made for the difference of vapor pressures of HTO and H2O. The effect of HTO adsorbed on chamber walls and electrodes was eliminated from the final result. Using Gerbes data on the number of electron volts to produce an ion pair in air, agreement obtained between the measured sourc… more
Date: July 23, 1953
Creator: Myers, I. T.
open access

The Less Familiar Elements in the Atomic Energy Program

Description: Many factors are responsible for the rapid growth of analytical chemistry during the past ten to fifteen years. One of the most important of these factors is the greatly increased significance to present day chemistry of many elements that in the recent past were principally chemical curiosities. Since the Atomic Energy program is concerned with many such elements, it is of interest to discuss the cause for this concern and the resulting effect on the field of analytical chemistry. A number … more
Date: October 12, 1953
Creator: Bushey, A. H.
open access

Microtitration of Free Acid in Uranyl Nitrate Solutions

Description: The approaches to the solution of the problem of removing or nullifying the effect of the hydrolysis of uranyl ion on acid titrations were: 1) use of a complexing agent and titration technique suitable for micro samples; 2) addition of a reagent that reacts with uranium to release 1 or 2 equivalents of acid per mole of uranium present (this permits correcting the titration value for the acid contributed by the uranium, or conversely permits an alkimetric titration of uranium); 3) separation of… more
Date: October 1, 1953
Creator: Carson, W. N., Jr.
open access

Monitoring Thermal and Resonance Neutron Flux

Description: The monitoring of thermal and resonance neutron flux in a thermal reactor having high flux over periods of time from 1 to 12 months using think Co foils is considered. Special attention is paid to the many correction factors to be applied to the activation data; neutron temperature, effective cadmium cutoff energy, burnout of Co59 and Co60, and decay of Co60. Results on a homogeneity test of 10 mil, 0.08% Co-A1 alloy foils is given.
Date: August 17, 1953
Creator: Heineman, R. E.
open access

Multiplication of Enriched Loading in Exponential Pile

Description: This report refutes earlier calculations made in the flux level of exponential piles. The results of the earlier calculations made on subcritical assemblies using critical assembly equations are in error. The calculations used in this report were more successful.
Date: September 28, 1953
Creator: Farrand, W. B. & Lloyd, R. C.
open access

Neutron Diffusion and Random Walk

Description: The following report analyzes random walks and whether or not they can be used to shed any light on problems of neutron diffusion.
Date: February 5, 1953
Creator: Duvall, G. E.
open access

Outgassing Tests of Uranium Slugs

Description: During the canning of slugs for Production Test 313-105-3-M, a high number of rejects were caused by gas voids in the A1-S1 bonding layer. Since the heat treatment of the slugs in a molten salt bath resulted in a chemically altered surface, an investigation was made to determine the volume of gas evolved from salt-bath heat-treated slugs as compared to other types of slugs. This test was designed as a preliminary test to determine if there were a significant differences.
Date: May 27, 1953
Creator: Johnson, H. A.
open access

Physical Properties of Tributylphosphate-Diluent Solutions

Description: In connection with the study of aqueous-tributyIphosphate (TBP) systems, the study of the interactions of various diluents with the TBP has been extended. The diluents used were mineral oil, Amsco 125-90W, dodecane, n-hexane, cyclohexane, benzene, n-octyl bromide, carbon tetrachloride, chloroform and pentachloroethane. The solubility of TBP in water from solutions of these diluents and the solubility of water in the organic phase was determined. For the paraffin hydrocarbons as diluents the … more
Date: September 1, 1953
Creator: Johnson, W. F. & Dillon, R. L.
open access

Plutonium Trichloride: Preparation by Reaction with Phosgene or Carbon Tetrachloride and Bomb Reduction to Metal

Description: Thirty gram patches of plutonium dioxide can be readily chlorinated by reaction with phosgene or carbon tetrachloride at temperatures of 350 and 450 C respectively. Plutonium trichloride prepared by either method can be reduced to the metal in a hermetically sealed bomb by reaction with calcium. On a twenty gram scale yields of approximately 97 per cent are obtained when a calcium-iodine booster is employed. It has been demonstrated that a method for reduction of plutonium trichloride to the… more
Date: December 3, 1953
Creator: Tolley, W. B.
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