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Analysis of X-ray Powder Diffraction Data on Crystalline Uranium Hexafluoride.

Description: From introduction: "The concluding remarks of the report on the electron diffraction study of UF6 suggest two alternate explanations for the apparent discrepancy between the structure proposed for this compound as deduced from X-ray diffraction work on single crystals and from the electron diffraction investigation of the vapor. The second explanation is based on the premise that the difference may be due to essentially unlike methods of treating the diffraction data. In this report we shall an… more
Date: March 5, 1946
Creator: Bauer, S. H. (Simon Harvey), 1911- & Palter, H.
open access

Argonne National Laboratory Biology Division Quarterly Report: August to October, 1946

Description: From introductory paragraph: "This is the first quarterly report of the Biology Division of the Argonne National Laboratory. During the three-month period covered by this report, a large share of the time of many investigators has been spent in collating work done under the Biology Section of the Metallurgical laboratory for publication in the Plutonium Project Record. The large amount of work done under wartime pressure has made this, as in other divisions and projects, an important part of th… more
Date: November 21, 1946
Creator: Bruss, Austin M.
open access

Autoxidation of Uranous Salts in Water Solution

Description: From introduction: "The fact that tetravalent uranium either in the form of solutions of its salts or, in some cases, in the dry state is readily oxidized by gaseous oxygen, has been observed by various investigators. A quantitative study of this reaction appeared to be desirable as a means of learning more about the nature of the ionic species present in uranous solutions. It was also of potential value in determining the importance of autoxidation as an undesirable side reaction involved in t… more
Date: April 20, 1946
Creator: Nichols, Ambrose R., Jr.
open access

The Beta-Gamma Hand and Foot Counters

Description: Abstract: This is basically a counting rate meter, with an alarm circuit, operating from four GM tubes as the detecting elements. The Hand Counter comprises four logarithmic counting rate meters working from four GM tubes mounted individually, with associated electronic circuits, in suitable shields with a metal mesh type of window. Both sides of both hands are sampled simultaneously. In the Foot Counter, two GM tubes are separately and mounted in a suitable mesh window shielded with the el… more
Date: May 1946
Creator: Bradley, W. H.
open access

The Bragg Reflection of Neutrons by a Single Crystal

Description: From cover page: This document has been assigned the above MDDC (Manhattan District Declassification) number, as given in the List of Declassified Documents issued semi-monthly by the Research Division, Manhattan District. In the case of Los Alapnos reports, LADC (Los Alamos Declassification) numbers are listed on the title page if known. This declassified document may differ materially from the original classified document by reason of deletions necessary to accomplish declassification. Hence,… more
Date: June 14, 1946
Creator: Zinn, Walter H.
open access

The Chemical Effects of Nuclear Transformations

Description: This technical report is divided into two sections addressing two different chemical effects of nuclear transformations. The first section discusses the beta decay of lanthanum to cerium. The second section discusses the beta decay of selenium to bromine.
Date: June 6, 1946
Creator: Coryell, Charles D. (Charles Du Bois), 1912-1971; Gest, H.; Edwards, R. R. & Davies, T. H.
open access

Comparative Effectiveness and Additivity of Fission Neutrons Gamma Rays and Beta Rays of Drosphila Eggs

Description: From abstract: "Some investigations have been made to ascertain the similarity of the mechanism of action of radiation which are different in their specific ionization. A suggested approach was to determine if the energies absorbed from the different types of radiation are additive in their lethal effects on biological objects. In an attempt to determine the additivity of ionizing radiation various dose combinations of fast neutrons, gamma rays and beta rays were administered to Drosophila eggs… more
Date: February 1946
Creator: Stapleton, G. E. & Zirkle, Raymond E. (Raymond Elliot), 1902-1988
open access

Contributions to the Radiochemistry of 104 day Y88.

Description: From introductory paragraph: "The study of the counting techniques of gamma-emitting radioisotopes is of a great deal of interest to workers in the field of radiochemistry. Of particular interest to the long-lived gamma emitting isotope of yttrium which is commonly prepared by a deuteron bombardment of strontium and is reported to decay by K-capture. This isotope, which is of interest in the fields of biochemistry and metallurgy was tentatively assigned to mass 86. Since a 2.0 hour activity was… more
Date: September 20, 1946
Creator: Overman, Ralph T.
open access

Crystal Structure Studies of the System NaF-UF4, NaF-ThF4 and NaF-LaF3

Description: Abstract: In the NaF-UF4 system the following intermediate phases have been found: NaUF5, -Na2UF6, -Na2UF6 and NacUF7. NaLaF4 is the only intermediate phase observed in the system NaF-LaF3. In the course of an incomplete study of the system NaF-ThF4 the phases NaTh2F9, -Na2ThF6, -Na2ThF6 and Na4ThF8 have been observed. Crystal structure data are given for all the phases.
Date: August 1946
Creator: Zachariasen, William H. (William Houlder), 1906-1979
open access

Determination of Oxygen in Uranium by Vacuum Fusion

Description: From abstract: "An apparatus for analysis of metal samples for oxygen content is described. Vasuum [sic] fusion in a graphite crucible which is insulated by porous carbon in an all pyrex glass apparatus is used to remove the oxygen as carbon monoxide. Temperatures over 2000°C. are attainable with a 6 K.V.A. Ajax converter for induction heating. Successful operation depended upon a preliminary vacuum heating of the carbon parts at 2100°C. to remove hydrocarbon tars so that cracking of the pyrex … more
Date: 1946
Creator: Brewer, Leo, 1919-2005
open access

The Effect of Age on the Radiosensitivity of Mice

Description: Abstract: Mice of different ages ranging from 1.5 to 12 months have been exposed to gamma rays in an effort to determine the change in radiosensitivity with age. The dose necessary to cause 50% killing was determined for each age group and sex. No change in sensitivity with age was observed with either sex, although the experimental error in the case of the males was quite large. The females were found to be more resistant than the males.
Date: April 8, 1946
Creator: Curtis, H. J.; Zirkle, Raymond E. (Raymond Elliot), 1902-1988; Anderson, Ernest C., 1920-2013 & Riley, E. F.
open access

The Effect of Clay on the Intestinal Absorption of Strontium

Description: From abstract: "Rats have been fed active strontium which was adsorbed on clay, while their controls were fed the same amount of active strontium in aqueous solution. There was no significant difference in the amount deposited in the skeleton between the two groups, and it is concluded that if ions are adsorbed on inert material, they will be eluted during their passage through the gastrointestinal tract."
Date: January 21, 1946
Creator: Curtis, Howard J. (Howard James), 1906-
open access

The Effects of Fast Neutrons on the Ability of Mice to Take Forced Exercise

Description: From abstract: "In an attempt to gain some insight into the physiological condition of mice surviving massive doses of radiation, a study of their vitality was undertaken. It was assured that the ability of these animals to do forced work would be a measure of their vitality, Stimulating exposed animals to run in exercise wheels to their fullest capacity, has resulted in a demonstration of a striking vitality less during a post-irradiative period, when no other effects are demonstrable by gross… more
Date: August 22, 1946
Creator: Stapleton, G. K. & Curtis, H. J.
open access

Electrolytic Reduction of Uranyl Ion

Description: From introduction: "Due to the hydrogen overvoltage at the surface of a mercury cathode, uranium solutions is hydrochloric acid may be reduced not only to the tetravalent state, but until considerable trivalent uranium is formed. Other metallic ions act as oxidation-reduction catalysts as well as being reduced themselves. The following paper is a study of the various reactions taking place in solution and at the surface of the cathode."
Date: May 27, 1946
Creator: Nichols, Ambrose R., Jr.
open access

Fluorescence Analysis for Uranium

Description: From abstract: "An adaptation of a colorimeter for the rapid estimation of small amounts of uranium to ± 5% by fluorescence of a sodium fluoride bead or fluoride-carbonate melt is described. Solutions containing from 0.1 to 1000 micrograms per milliliter may be tested directly. The limit of visual detection on a 20 mg. bead is about 0.0003 microgram of uranium. A periodic chart of interferences is presented. The strangest interferences center around the latter parts of each transition series o… more
Date: 1946
Creator: Zebroski, E. L.; Newton, T. W. (Thomas William), 1923- & Ripple, F. T.
open access

The Geochemistry of Columbium and Tantalum

Description: From abstract: "This is a review, with annotated bibliography, of the mode of occurrence of the elements columbium and tantalum. It is not a list of specific ore deposits, but a summary of the types of minerals and rocks in which these elements have been reported to occur. In addition, the unpublished spectrographic studies of the Geological Survey are summarized, best sources for columbium and tantalum are indicated, and suggestions are made for further investigation."
Date: June 1946
Creator: Fleischer, Michael, 1908-1998 & Harder, James O.
open access

Geochemistry of Germanium

Description: From abstract: "This is a review, with annotated bibliography, of the mode of occurrence of the element germanium. It is not a list of specific ore deposits, but a summary of the types of minerals and rocks in which germanium has been reported to occur. Best sources for germanium are indicated, based on the data in the literature and on the unpublished spectrographic studies of the Geological Survey on mill and smelter products. Suggestions are made for further investigations."
Date: 1946
Creator: Fleischer, Michael, 1908-1998 & Harder, James O.
open access

The Geochemistry of Indium

Description: Abstract" This is a review, with annotated bibliography, of the mode of occurrence of the element indium. It is not a list of specific ore deposits, but a summary of the types of minerals and rocks in which indium has been reported to occur. In addition, the unpublished spectrographic studies of the Geological Survey on mill and smelter products are summarized, best sources of indium are indicated, and suggestions are made for further investigations. Indium has been found to occur most abund… more
Date: June 1946
Creator: Fleischer, Michael, 1908-1998 & Harder, James Otto.
open access

Infrared Spectrum of Benzene

Description: From abstract: "Benzene shows weak absorption bands in the 3 aliphatic C-Z region of the spectrum. The peaks of these bands are at 3.439, 3.459, 3.504, and 3.545."
Date: 1946
Creator: Flanagan, John; Gardner, R.; McKee, Frances & Schlegel, Richard, 1913-
open access

Inorganic Separations Using Ion Exchange

Description: From summary: "In previous project work, dilute mixtures of inorganic cations in aqueous solution have been concentrated by adsorption of the cations on a synthetic resin and they have been fractionated by selective desorption of the cations from the resin. In this report..the general procedure used in chemical separation, the equipment used, and the theory of the exchange equilibria and of the reaction rates are presented."
Date: August 29, 1946
Creator: Peterson, H. D.
open access

A Mass Spectrograph for the Analysis of Fission Product Mixtures

Description: From introduction: "The analysis of mixtures of fission products with a mass spectrograph offers certain advantages. A chemical separation of the fission products found in the solution at Hanford is not necessary with the mass spectrograph technique. A sample of the mixtures can be placed on the sample holder and then the sample holder is mounted in the mass spectrograph. This reduces the amount of handling of the active solutions to one relatively simple and short operation. The health hazards… more
Date: June 12, 1946
Creator: Lewis, Lloyd G., 1917-
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