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  Partner: UNT Libraries
 Decade: 2000-2009
 Degree Discipline: Engineering Technology
 Collection: UNT Theses and Dissertations
Effects of Thickness and Indenter Tip Geometry in Nanoindentation of Nickel Films

Effects of Thickness and Indenter Tip Geometry in Nanoindentation of Nickel Films

Access: Use of this item is restricted to the UNT Community.
Date: May 2004
Creator: Parakala, Padma
Description: Nanoindentation has become a widely used technique to measure the mechanical properties of materials. Due to its capability to deform materials in micro- and nano-scale, nanoindentation has found more applications in characterizing the deformation behavior and determining the mechanical properties of thin films and coatings. This research deals with the characterization of samples received from Center for Advanced Microstructures and Devices (CAMD) and Integran Technologies Inc., Toronto, Canada and the objective of this investigation was to utilize the experimental data obtained from nanoindentation to determine the deformation behavior, mechanical properties of thin films on substrates and bulk materials, and the effect of geometrically different indenters (Berkovich, cubecorner, and conical). X-ray diffraction (XRD), transmission electron microscope (TEM), scanning electron microscopy (SEM), and atomic force microscopy (AFM) analysis were performed on these materials to determine the crystal orientation, grain size of the material, and also to measure any substrate effects like pile-up or sin-in respectively. The results indicate that indentation size effect (ISE) strongly depends on shape of the indenter and less sensitive to penetration depth where as the hardness measurements depends on shape of indenter and depth of penetration. There is a negligible strain rate dependency of hardness at deeper depths ...
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Evaluation of dynamic and static electrical characteristics for the DY8 and YI8 process gallium diodes in comparison to the DI8 process boron diodes.

Evaluation of dynamic and static electrical characteristics for the DY8 and YI8 process gallium diodes in comparison to the DI8 process boron diodes.

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Date: December 2006
Creator: Dhoopati, Swathi
Description: A rectifier is an electrical device, comprising one or more semiconductor devices arranged for converting alternating current to direct current by blocking the negative or positive portion of the waveform. The purpose of this study would be to evaluate dynamic and static electrical characteristics of rectifier chips fabricated with (a) DY8 process and (b) YI8 process and compare them with the existing DI8 process rectifiers. These new rectifiers were tested to compare their performance to meet or exceed requirements of lower forward voltages, leakage currents, reverse recovery time, and greater sustainability at higher temperatures compared to diodes manufactured using boron as base (DI8 process diodes) for similar input variables.
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FEM of nanoindentation on micro- and nanocrystalline Ni: Analysis of factors affecting hardness and modulus values.

FEM of nanoindentation on micro- and nanocrystalline Ni: Analysis of factors affecting hardness and modulus values.

Date: August 2005
Creator: Pothapragada, Raja Mahesh
Description: Nanoindentation is a widely used technique to measure the mechanical properties of films with thickness ranging from nanometers to micrometers. A much better understanding of the contact mechanics is obtained mostly through finite element modeling. The experiments were modeled using the software package Nano SP1 that is based on COSMOSM™ (Structural Research & Analysis Corp, www.cosmosm.com), a finite element code. The fundamental material properties affecting pile-up are the ratio of the effective modulus to yield stress Eeff/σ and the work hardening behavior. Two separate cases of work hardening rates were considered; one with no work hardening rate and other with a linear work hardening rate. Specifically, it is observed that pile up is large only when hf/hmax is close to one and degree of work hardening rate is small. It should also be noted that when hf/hmax < 0.7 very little pile-up is observed no matter what the work-hardening behavior of the material. When pile-up occurs the contact area is greater than that predicted by the experimental methods and both the hardness and modulus are overestimated. In this report the amount by which these properties are overestimated are studied and got to be around 22% approx. Bluntness of the tip ...
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Flow Accelerated Corrosion Experience at Comanche Peak Steam Electric Station

Flow Accelerated Corrosion Experience at Comanche Peak Steam Electric Station

Date: May 2008
Creator: Nakka, Ravi Kumar
Description: Flow accelerated corrosion (FAC) is a major concern in the power industry as it causes thinning of the pipes by the dissolution of the passive oxide layer formed on the pipe surface. Present research deals with comparing the protection offered by the magnetite (Fe3O4) versus maghemite (γ-Fe2O3) phases thickness loss measurements. Fourier transform infrared spectroscopy (FTIR) is used in distinguishing these two elusive phases of iron oxides. Representative pipes are collected from high pressure steam extraction line of the secondary cycle of unit 2 of Comanche Peak Steam Electric Station (CPSES). Environmental scanning electron microscopy (ESEM) is used for morphological analysis. FTIR and X-ray diffraction (XRD) are used for phase analysis. Morphological analysis showed the presence of porous oxide surfaces with octahedral crystals, scallops and "chimney" like vents. FTIR revealed the predominance of maghemite at the most of the pipe sections. Results of thickness measurements indicate severe thickness loss at the bend areas (extrados) of the pipes.
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FPGA Prototyping of a Watermarking Algorithm for MPEG-4

FPGA Prototyping of a Watermarking Algorithm for MPEG-4

Date: May 2007
Creator: Cai, Wei
Description: In the immediate future, multimedia product distribution through the Internet will become main stream. However, it can also have the side effect of unauthorized duplication and distribution of multimedia products. That effect could be a critical challenge to the legal ownership of copyright and intellectual property. Many schemes have been proposed to address these issues; one is digital watermarking which is appropriate for image and video copyright protection. Videos distributed via the Internet must be processed by compression for low bit rate, due to bandwidth limitations. The most widely adapted video compression standard is MPEG-4. Discrete cosine transform (DCT) domain watermarking is a secure algorithm which could survive video compression procedures and, most importantly, attacks attempting to remove the watermark, with a visibly degraded video quality result after the watermark attacks. For a commercial broadcasting video system, real-time response is always required. For this reason, an FPGA hardware implementation is studied in this work. This thesis deals with video compression, watermarking algorithms and their hardware implementation with FPGAs. A prototyping VLSI architecture will implement video compression and watermarking algorithms with the FPGA. The prototype is evaluated with video and watermarking quality metrics. Finally, it is seen that the video qualities ...
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Increasing the Dynamic Range of Audio THD Measurements Using a Novel Noise and Distortion Canceling Methodology

Increasing the Dynamic Range of Audio THD Measurements Using a Novel Noise and Distortion Canceling Methodology

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Date: May 2003
Creator: Dunipace, Richard Alan
Description: The objective of this study was to determine how a new experimental methodology for measuring Total-Harmonic-Distortion (THD) of operational amplifiers functioned when compared with two standard methodologies, and whether the new methodology offers any improvement in noise floor and dynamic range along with distortion canceling of the sine-wave source used in the testing. The new methodology (THD) is being tested against two standard methodologies: Spectral Analysis using a tuned receiver type Spectrum Analyzer with Notch Filter pre-processing, and a digitized Fast Fourier Transform (FFT) using Notch Filter pre-processing. The THD results appear to agree across all methodologies, and across all items of the sample within all methodologies, to within a percent or less. The distortion and noise canceling feature of the new methodology appeared to function as expected and in accordance with theory. The sample tested in the study consisted of thirty-five NE5534 operational amplifiers produced by Texas Instruments, Inc. and purchased from a local store. The NE5534 is a low-noise, low-distortion, operational amplifier that is widely used in industry and is representative of today's best audio amplifiers.
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Indoor Propagation Modeling at 2.4 GHz for IEEE 802.11 Networks

Indoor Propagation Modeling at 2.4 GHz for IEEE 802.11 Networks

Date: December 2005
Creator: Tummala, Dinesh
Description: Indoor use of wireless systems poses one of the biggest design challenges. It is difficult to predict the propagation of a radio frequency wave in an indoor environment. To assist in deploying the above systems, characterization of the indoor radio propagation channel is essential. The contributions of this work are two-folds. First, in order to build a model, extensive field strength measurements are carried out inside two different buildings. Then, path loss exponents from log-distance path loss model and standard deviations from log-normal shadowing, which statistically describe the path loss models for a different transmitter receiver separations and scenarios, are determined. The purpose of this study is to characterize the indoor channel for 802.11 wireless local area networks at 2.4 GHz frequency. This thesis presents a channel model based on measurements conducted in commonly found scenarios in buildings. These scenarios include closed corridor, open corridor, classroom, and computer lab. Path loss equations are determined using log-distance path loss model and log-normal shadowing. The chi-square test statistic values for each access point are calculated to prove that the observed fading is a normal distribution at 5% significance level. Finally, the propagation models from the two buildings are compared to validate the ...
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Investigation of the feasibility of non-invasive carbon dioxide detection using spectroscopy in the visible spectrum.

Investigation of the feasibility of non-invasive carbon dioxide detection using spectroscopy in the visible spectrum.

Date: December 2007
Creator: Marks, Damian
Description: Pulse oximeters are used in operating rooms and recovery rooms as a monitoring device for oxygen in the respiratory system of the patient. The advantage of pulse oximeters over other methods of oxygen monitoring is that they are easy to use and they are non-invasive, which means it is not necessary break the skin to extract blood for information to be obtained. The standard for the measurement of partial pressure of CO2 and O2 is an arterial blood gas analysis (ABG). However routine monitoring using this method on a continuous basis is impractical since it is slow, painful and invasive. Measuring carbon dioxide is critical to preventing ailments such as carbon dioxide poisoning or hypoxia. The problem is, currently there is no known effective non-invasive method for accurately measuring carbon dioxide in the body to properly assess the adequacy of ventilation. The objective of this study was to experimentally use spectroscopy in the visible spectrum and the principles of operation of a pulse oximeter to incorporate a method of non-invasive real-time carbon dioxide monitoring that is as quick and easy to use.
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Laser Cutting Machine: Justification of initial costs

Laser Cutting Machine: Justification of initial costs

Date: May 2001
Creator: Nagaraja, Dwarakish
Description: The Industrial Laser is firmly established in metalcutting as the tool of choice for many applications. The elevator division of Montgomery KONE Inc., in an effort to move towards quality, ontime, complete deliveries and 100% customer satisfaction, decided to invest in new equipment to improve manufacturing processes. A huge investment is proposed for a laser-cutting machine. It is the responsibility of Manufacturing Engineering to direct the management by justifying its benefits, which includes payback time and financial gains. Factors such as common line cutting, automated material handling system and cutting time were involved in justification of the initial cost of a laser-cutting machine. Comparative statistics on appropriate factors accurately determine and justify the initial cost of a laser-cutting machine.
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Linearity and monotonicity of a 10-bit, 125 MHz, segmented current steering digital to analog converter

Linearity and monotonicity of a 10-bit, 125 MHz, segmented current steering digital to analog converter

Date: May 2000
Creator: Bittle, Charles C.
Description: The purpose of this research is to determine the linearity and monotonicity of the THS5651IDW digital to analog converter (DAC), a prototype of the future Texas Instruments TLV5651, 10-bit, 125 MHz communication DAC. Testing was conducted at the Texas Instruments facility on Forest Lane, Dallas, Texas. Texas Instruments provided test equipment, software and laboratory space to obtain test data. Analysis of the data found the DAC to be monotonic since the magnitude of the differential nonlinearity (DNL) was less than ± 1 least significant bit (LSB) and the integral nonlinearity (INL) was less than ± 0.5 LSB. The study also showed that the DAC has primarily negative DNL although the DNL is well within the desired specification.
Contributing Partner: UNT Libraries