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  Access Rights: Public
  Partner: UNT Libraries
 Department: Department of Engineering Technology
 Decade: 2000-2009
 Collection: UNT Theses and Dissertations
Characterization of boron nitride thin films on silicon (100) wafer.

Characterization of boron nitride thin films on silicon (100) wafer.

Date: August 2007
Creator: Maranon, Walter
Description: Cubic boron nitride (cBN) thin films offer attractive mechanical and electrical properties. The synthesis of cBN films have been deposited using both physical and chemical vapor deposition methods, which generate internal residual, stresses that result in delamination of the film from substrates. Boron nitride films were deposited using electron beam evaporation without bias voltage and nitrogen bombardment (to reduce stresses) were characterize using FTIR, XRD, SEM, EDS, TEM, and AFM techniques. In addition, a pin-on-disk tribological test was used to measure coefficient of friction. Results indicated that samples deposited at 400°C contained higher cubic phase of BN compared to those films deposited at room temperature. A BN film containing cubic phase deposited at 400°C for 2 hours showed 0.1 friction coefficient.
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Cold-Formed Steel Bolted Connections without Washers on Oversized and Slotted Holes

Cold-Formed Steel Bolted Connections without Washers on Oversized and Slotted Holes

Date: May 2009
Creator: Sheerah, Ibraheem
Description: The use of the cold-formed steel sheet bolted connections without washers is so significant; however, the North American Specifications for the Design of Cold Formed Steel Structural Members, NASPEC, doesn't provide provisions for such connections. The bearing failure of sheet and the shear failure of sheet were considered in this study. For the sheet shear strength, it was found that the NASPEC (2007) design provisions can be used for oversized holes in both single and double shear configurations and for the double shear connections on short slotted holes. For the sheet bearing strength, a new design method was proposed to be used for low and high ductile steel sheets. The method was compared with the NASPEC and the University of Waterloo approach. Washers were still required for single shear connections on short slotted holes. Besides, connections using ASTM A325 bolts yielded higher bearing strength than connections using ASTM A307 bolts.
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Computer virus spread containment using feedback control.

Computer virus spread containment using feedback control.

Date: December 2004
Creator: Yelimeli Guruprasad, Arun
Description: In this research, a security architecture based on the feedback control theory has been proposed. The first loop has been designed, developed and tested. The architecture proposes a feedback model with many controllers located at different stages of network. The controller at each stage gives feedback to the one at higher level and a decision about network security is taken. The first loop implemented in this thesis detects one important anomaly of virus attack, rate of outgoing connection. Though there are other anomalies of a virus attack, rate of outgoing connection is an important one to contain the spread. Based on the feedback model, this symptom is fed back and a state model using queuing theory is developed to delay the connections and slow down the rate of outgoing connections. Upon implementation of this model, whenever an infected machine tries to make connections at a speed not considered safe, the controller kicks in and sends those connections to a delay queue. Because of delaying connections, rate of outgoing connections decrease. Also because of delaying, many connections timeout and get dropped, reducing the spread. PID controller is implemented to decide the number of connections going to safe or suspected queue. Multiple ...
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Cost savings realized through proper sizing of an excessive instrument air system.

Cost savings realized through proper sizing of an excessive instrument air system.

Date: December 2003
Creator: Condron, Ewell D.
Description: The purpose of this research was to determine if installing a smaller air compressor could reduce the electrical usage of a large semiconductor manufacturing plant. A 200 horsepower Atlas Copco compressor was installed with the existing 500 horsepower Ingersoll-Rand compressors. Testing was conducted during the regular manufacturing process at MEMC Southwest in Sherman, Texas. Analysis of the data found that installing the new compressor could reduce electrical consumption. The study also found there are specific operational setpoints that allow the compressor to operate more efficiently.
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Design and validation of an automated multiunit composting system.

Design and validation of an automated multiunit composting system.

Date: December 2009
Creator: Pickens, Mark Everett
Description: This thesis covers the design of an automated multiunit composting system (AMUCS) that was constructed to meet the experimental apparatus requirements of the ASTM D5338 standard. The design of the AMUCS is discussed in full detail and validated with two experiments. The first experiment was used to validate the operation of the AMUCS with a 15 day experiment. During this experiment visual observations were made to visually observe degradation. Thermal properties and stability tests were performed to quantify the effects of degradation on the polymer samples, and the carbon metabolized from the degradation of samples was measured. The second experiment used the AMUCS to determine the effect of synthetic clay nanofiller on the aerobic biodegradability behavior of poly (3-hydroxybutyrate-co-3-hydroxyvalerate).
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Determination of the shelf life of aluminum electrolytic capacitors.

Determination of the shelf life of aluminum electrolytic capacitors.

Date: May 2002
Creator: Wynne, Edward McFaddin
Description: The aluminum electrolytic capacitor is used extensively in the electric utility industry. A factor limiting the storage of spare capacitors is the integrity of the aluminum oxide dielectric, which over time breaks down contributing to a shelf life currently estimated at one nuclear power electric generating station to be approximately five years. This project examined the electrical characteristics of naturally aged capacitors of several different styles to determine if design parameters were still within limits. Additionally, the effectiveness of a technique known as “Reforming” was examined to determine its impact on those characteristics.
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Effect of Amines as Corrosion Inhibitors for a Low Carbon Steel in Power Industry

Effect of Amines as Corrosion Inhibitors for a Low Carbon Steel in Power Industry

Date: December 2004
Creator: Díaz, Jorge G.
Description: Commonly used amines in power industry, including morpholine, DBU (1,8-diazabicyclo[5.4.0]undec-7-ene), and DMA (dimethylallylamine) were evaluated for their effect on AISI 1018 steel at 250oF. Samples were exposed to an autoclave containing amine added aqueous solution at pH of 9.5 for 1, 2, 4, 6, 8, and 12 hours. Morphology studies were carried using scanning electron microscope (SEM), phase analysis was done utilizing Fourier transform infrared spectroscopy (FTIR), and weight loss was performed to assess kinetics of oxidation. Control samples showed the highest metal dissolution rate. DBU showed the best performance in metal protection and SEM indicated the presence of a free-crack layer formed by fine particles in that set. FTIR showed that DBU apparently favored the formation of magnetite. It is believed that fine particles impede intrusion of aggressive ions into the metal surface by forming a barrier layer. FTIR demonstrated that DMA formed more oxyhydroxides, whereas morpholine presented magnetite to hematite transformation as early as 2 hours. SEM revealed that control and DMA produced acicular particles characteristic of oxyhydroxides while morpholine and DBU presented more equiaxed particles.
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Effects of a surface engineered metallic coating on elastomeric valve stem seal leakage

Effects of a surface engineered metallic coating on elastomeric valve stem seal leakage

Date: December 2000
Creator: Taylor, John Abner
Description: Valve stem seal leakage is a major source of fugitive emissions, and controlling these emissions can result in added expense in leak detection and repair programs. Elastomeric O-rings can be used as valve stem seals, and O-ring manufacturers recommend lubrication of elastomeric seals to prevent damage and to assure proper sealing. In this research, a metallic coating was applied as a lubricant using a vacuum vapor deposition process to the surface of elastomeric valve stem seals. Valve stem leak measurements were taken to determine if the coated O-rings, alone or with the recommended lubrication, reduced valve stem seal leakage. This research determined that the metallic coating did not reduce valve stem leakage.
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Effects of minimum quantity lubrication in drilling 1018 steel.

Effects of minimum quantity lubrication in drilling 1018 steel.

Date: December 2008
Creator: Shaikh, Vasim
Description: A common goal for industrial manufacturers is to create a safer working environment and reduce production costs. One common method to achieve this goal is to drastically reduce cutting fluid use in machining. Recent advances in machining technologies have made it possible to perform machining with minimum-quantity lubrication (MQL). Drilling takes a key position in the realization of MQL machining. In this study the effects of using MQL in drilling AISI 1018 steel with HSS tools using a vegetable based lubricant were investigated. A full factorial experiment was conducted and regression models were generated for both surface finish and hole size. Lower surface roughness and higher tool life were observed in the lowest speed and feed rate combination.
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Factors influencing horizontal cracking in continuously reinforced concrete pavements (CRCP).

Factors influencing horizontal cracking in continuously reinforced concrete pavements (CRCP).

Date: August 2008
Creator: Sudoi, Elias K.
Description: This research presents the results on an experimental investigation to identify the significant factors influencing horizontal cracking in continuously reinforced concrete pavements (CRCP). An in-depth analysis of the microstructure, morphological characteristics of the interfacial transition zone (ITZ) and the observation of cracking using the environmental scanning electron microscope (ESEM) was done. Characterization of oxides using Fourier transform infrared spectroscopy (FTIR) and electron dispersive x-ray spectroscopy (EDS) was also performed. Water to cement ratio (w/c) and rebar temperature had a significant influence on the rebar-concrete bond strength. The 28-day shear strength measurements showed an increase in rebar-concrete bond strength as the water to cement ratio (w/c) was reduced from 0.50 to 0.40. There was a reduction in the peak pullout load as the temperature increased from 14oF to 252oF for the corroded and non-corroded rebar experiments. The corroded rebar pullout test results showed a 20-50 % reduction in bond strength compared to the non-corroded rebars. FTIR measurements indicated a presence of lepidocrocrite (γ -FeOOH) and maghemite (γ -Fe2O3) on the ITZ. ESEM images showed the existence of microcracks as early as three days after casting with the bridging of these cracks between coarse aggregate locations in the interfacial zone propagating through ...
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