Alkali-silica reaction (ASR) in cement is a major contributor to failure of cement structures around the world, causing increased repair costs and possible rebuild expenses. Alkali levels are indicative of the potential for ASR and are therefore measured and quantified. A linear correlation relating cement alkali concentration measured by X-ray fluorescence spectroscopy (XRF) and peak ratio measured by Fourier transform infrared spectroscopy (FTIR) is developed. Regression analysis of plots correlating alkali content measured by FTIR absorption band (750 cm-1/923 cm-1) ratio versus equivalent alkali (Na2O)e (%Na2O + 0.658 % K2O) quantified by XRF show linear correlation coefficient, R2, of 0.97. Results of this investigation are discussed in terms of microstructural disorder coefficient Cd which is a reactivity criterion for ASR-susceptible aggregates proposed by Bachiorrini [31]. XRF is a popular technique for alkali quantification but FTIR is faster, safer, and less expensive technique compared to XRF. Portable instrumentation is available for both techniques but FTIR systems are less expensive.
In cold-formed steel (CFS) construction, bolted connections without washers for either oversized or slotted holes may significantly expedite the installation process and lower the cost. However, the North American Specification (AISI S100, 2007) for the Design of Cold-Formed Steel Structural Members requires washers to be installed in bolted connections with oversized or slotted holes. A research project (Phase 1) sponsored by American Iron and Steel Institute (AISI) was recently completed at the University of North Texas (UNT) that investigated the performance and strength of bolted CFS connections with oversized and slotted holes without using washers. The research presented in this thesis is the Phase 2 project in which the bolted CFS connections were studied in a broader respect in terms of the failure mechanism, the material thickness, and the hole configurations. Single shear and double shear connections without washers using oversized holes, oversized combined with standard or slotted holes were experimentally examined. Combined with Phase 1 results, the Phase 2 gives a comprehensive evaluation of the behavior and strength of bolted CFS connections with oversized and slotted holes without using washers. Revisions to the existing AISI North American Specification requirements for bolted connections are proposed to account for the reduction in the connection strength caused by the oversized and slotted hole configurations without washers. Specific LRFD and LSD resistance factors and ASD safety factors for different hole configurations in terms of the new proposed methods were presented.
The use of the cold-formed steel sheet bolted connections without washers is so significant; however, the North American Specifications for the Design of Cold Formed Steel Structural Members, NASPEC, doesn't provide provisions for such connections. The bearing failure of sheet and the shear failure of sheet were considered in this study. For the sheet shear strength, it was found that the NASPEC (2007) design provisions can be used for oversized holes in both single and double shear configurations and for the double shear connections on short slotted holes. For the sheet bearing strength, a new design method was proposed to be used for low and high ductile steel sheets. The method was compared with the NASPEC and the University of Waterloo approach. Washers were still required for single shear connections on short slotted holes. Besides, connections using ASTM A325 bolts yielded higher bearing strength than connections using ASTM A307 bolts.
This thesis covers the design of an automated multiunit composting system (AMUCS) that was constructed to meet the experimental apparatus requirements of the ASTM D5338 standard. The design of the AMUCS is discussed in full detail and validated with two experiments. The first experiment was used to validate the operation of the AMUCS with a 15 day experiment. During this experiment visual observations were made to visually observe degradation. Thermal properties and stability tests were performed to quantify the effects of degradation on the polymer samples, and the carbon metabolized from the degradation of samples was measured. The second experiment used the AMUCS to determine the effect of synthetic clay nanofiller on the aerobic biodegradability behavior of poly (3-hydroxybutyrate-co-3-hydroxyvalerate).
This research presents the results on an experimental investigation to identify the effect of polyphosphoric acid (PPA) on aging characteristics of an asphalt binder. Addition of PPA to asphalt binders is said to improve performance of flexible pavements. Asphalt binder PG 64-22 in modified and unmodified conditions was subjected to aging in the laboratory using a regular oven and also simulated short term aging using rolling thin film oven (RTFO) test. Aging experiments were conducted to analyze the extent of oxidation in terms of changes in molecular structure of the asphalt binder. These changes were appraised using Fourier transform infrared (FTIR) spectroscopy, dynamic shear rheometer (DSR), and epifluorescence microscopy tests. FTIR was used to determine the changes in major bands with addition of PPA. Stiffness and viscoelastic behaviors of asphalts were determined from the DSR test. The stiffness is measured by calculating the shear modulus, G* and the viscoelastic behavior is measured by calculating the phase angle, sin δ. Epifluorescence microscopy is a tool used to study properties of organic or inorganic substances. The morphological characteristics of PPA modified asphalt samples were observed through epifluorescence microscopy. Epifluorescence microscopy reveals the polymer phase distribution in the asphalt binders. Results of this investigation show PPA addition to asphalt binders improve G*/sin δ characteristics of asphalt binders. In addition, presence of PPA in polymer containing asphalt did not adversely affect aging of the binders.
A common goal for industrial manufacturers is to create a safer working environment and reduce production costs. One common method to achieve this goal is to drastically reduce cutting fluid use in machining. Recent advances in machining technologies have made it possible to perform machining with minimum-quantity lubrication (MQL). Drilling takes a key position in the realization of MQL machining. In this study the effects of using MQL in drilling AISI 1018 steel with HSS tools using a vegetable based lubricant were investigated. A full factorial experiment was conducted and regression models were generated for both surface finish and hole size. Lower surface roughness and higher tool life were observed in the lowest speed and feed rate combination.
The mechanical properties of a polymer represent the critical characteristics to be considered when determining the applications for it. The same polymer processed with different methods can exhibit different mechanical properties. The purpose of this study is to investigate the difference in mechanical properties of the selected polymers caused by different processing techniques and conditions. Three polymers were studied, including low density polyethylene (LDPE), polypropylene (PP), and NEXPRENE® 1287A. Samples were processed with injection molding and compression molding under different processing condition. Tensile and DMA tests were performed on these samples. The acquired data of strain at break from the tensile tests and storage modulus from the DMA were utilized to calculate brittleness. Calculated brittleness values were used to perform analysis of variance (ANOVA) to investigate the statistical significance of the processing technique and condition. It was found that different processing techniques affect the brittleness significantly. The processing technique is the major factor affecting brittleness of PP and NEXPRENE, and the processing temperature is the major factor affecting brittleness of LDPE.
This research presents the results on an experimental investigation to identify the effects of rebar temperature, fly ash and water to cement ratio on concrete porosity in continuously reinforced concrete pavements (CRCP). Samples were cast and analyzed using pullout tests. Water to cement ratio (w/c) and rebar temperature had a significant influence on the rebar-concrete bond strength. The 28-day shear strength measurements showed an increase in rebar-concrete bond strength as the water to cement ratio (w/c) was reduced from 0.50 to 0.40 for both fly ash containing and non fly ash control samples. There was a reduction in the peak pullout load as the rebar surface temperature increased from 77o F to 150o F for the cast samples. A heated rebar experiment was performed simulating a rebar exposed to hot summer days and the rebar cooling curves were plotted for the rebar temperatures of 180o F - 120o F. Fourier transform infrared spectroscopy was performed to show the moisture content of cement samples at the rebar-concrete interface. Mercury intrusion porosimetry test results on one batch of samples were used for pore size distribution analysis. An in-depth analysis of the morphological characteristics of the rebar-concrete interface and the observation of pores using the scanning electron microscope (SEM) was done.
Smart structures are relevant and significant because of their relevance to phenomena such as hazard mitigation, structural health monitoring and energy saving. Electrical resistance could potentially serve as an indicator of structural well-being or damage in the structure. To this end, the development of a microprocessor-based automated resistance measurement system with customized GUI is desired. In this research, a nodal electrical resistance acquisition circuit (NERAC) system was designed. The system hardware interfaces to a laptop, which houses a customized GUI developed using DAQFactory software. Resistance/impedance was measured using DC/AC methods with four-point probes technique, on three substrates. Baseline reading before damage was noted and compared with the resistance measured after damage. The device was calibrated and validated on three different substrates. Resistance measurements were taken from PVDF samples, composite panels and smart concrete. Results conformed to previous work done on these substrates, validating the effective working of the NERAC device.
This research presents the results on an experimental investigation to identify the significant factors influencing horizontal cracking in continuously reinforced concrete pavements (CRCP). An in-depth analysis of the microstructure, morphological characteristics of the interfacial transition zone (ITZ) and the observation of cracking using the environmental scanning electron microscope (ESEM) was done. Characterization of oxides using Fourier transform infrared spectroscopy (FTIR) and electron dispersive x-ray spectroscopy (EDS) was also performed. Water to cement ratio (w/c) and rebar temperature had a significant influence on the rebar-concrete bond strength. The 28-day shear strength measurements showed an increase in rebar-concrete bond strength as the water to cement ratio (w/c) was reduced from 0.50 to 0.40. There was a reduction in the peak pullout load as the temperature increased from 14oF to 252oF for the corroded and non-corroded rebar experiments. The corroded rebar pullout test results showed a 20-50 % reduction in bond strength compared to the non-corroded rebars. FTIR measurements indicated a presence of lepidocrocrite (γ -FeOOH) and maghemite (γ -Fe2O3) on the ITZ. ESEM images showed the existence of microcracks as early as three days after casting with the bridging of these cracks between coarse aggregate locations in the interfacial zone propagating through the mortar.
Analog technology has been around for a long time. The use of analog technology is necessary since we live in an analog world. However, the transmission and storage of analog technology is more complicated and in many cases less efficient than digital technology. Digital technology, on the other hand, provides fast means to be transmitted and stored. Digital technology continues to grow and it is more widely used than ever before. However, with the advent of new technology that can reproduce digital documents or images with unprecedented accuracy, it poses a risk to the intellectual rights of many artists and also on personal security. One way to protect intellectual rights of digital works is by embedding watermarks in them. The watermarks can be visible or invisible depending on the application and the final objective of the intellectual work. This thesis deals with watermarking images in the discrete wavelet transform domain. The watermarking process was done using the JPEG2000 compression standard as a platform. The hardware implementation was achieved using the ALTERA DSP Builder and SIMULINK software to program the DE2 ALTERA FPGA board. The JPEG2000 color transform and the wavelet transformation blocks were implemented using the hardware-in-the-loop (HIL) configuration.
This research lays the foundation of a highly simplified maskless micro-fabrication technique which involves incorporation of laser direct writing technique combined with fountain pen based micro-patterning method to fabricate polymer-based Mach-Zehnder interferometer sensor arrays' prototype for chemical/biological sensing applications. The research provides methodology that focuses on maskless technology, allowing the definition and modification of geometric patterns through the programming of computer software, in contrast to the conventional mask-based photolithographic approach, in which a photomask must be produced before the device is fabricated. The finished waveguide sensors are evaluated on the basis of their performance as general interferometers. The waveguide developed using the fountain pen-based micro-patterning system is compared with the waveguide developed using the current technique of spin coating method for patterning of upper cladding of the waveguide. The resulting output power profile of the waveguides is generated to confirm their functionality as general interferometers. The results obtained are used to confirm the functionality of the simplified micro-fabrication technique for fabricating integrated optical polymer-based sensors and sensor arrays for chemical/biological sensing applications.
In this research, monotonic and cyclic tests on cold-formed steel shear walls sheathed with steel sheets on one side were conducted to (1) verify the published nominal shear strength for 18-mil and 27-mil steel sheets; and (2) investigate the behavior of 6-ft. wide shear walls with multiple steel sheets. In objective 1: this research confirms the discrepancy existed in the published nominal strength of 27-mil sheets discovered by the previous project and verified the published nominal strength of 18 mil sheet for the wind design in AISI S213. The project also finds disagreement on the nominal strength of 18-mil sheets for seismic design, which is 29.0% higher than the published values. The research investigated 6-ft. wide shear wall with four framing and sheathing configurations. Configuration C, which used detailing, could provide the highest shear strength, compared to Configurations A and B. Meanwhile, the shear strength and stiffness of 2-ft. wide and 4-ft. wide wall can be improved by using the seismic detailing.
In the cold-formed steel construction, the oriented strand board is a common material for shear wall sheathing. an OSB is made by using wood chips as raw materials that undergo high temperature pressing to create a multi-larger structure material. Due to the OSB having a high strength in shear, it is an important material used in the construction field. the thesis is trying to verify published nominal shear strength in AISI-213-07 in the first part. This objective has two parts: the first part is to verify nominal shear strength (Rn) for wind and other in-plane loads for shear wall. the second part is to verify nominal shear strength (Rn) for seismic and other in-plane loads for shear wall. Secondly, the thesis verifies the design deflection equation for nominal shear strength of CFS shear walls with OSB sheathing. the test specimens were divided into eight groups which trying to verify the design deflection equation that was published in AISI-213-07 standard.
Currently, ASHRAE has determined the zone method and modified zone method are appropriate calculation methods for materials with a high difference in conductivity, such as cold-formed steel (CFS) walls. Because there is currently no standard U-Factor calculation method for CFS walls, designers and code officials alike tend to resort to the zone method. However, the zone method is restricted to larger span assemblies because the zone factor coefficient is 2.0. This tends to overestimate the amount of surface area influenced by CFS. The modified zone method is restricted to C-shaped stud, clear wall assemblies with framing factors between 9 and 15%. The objective of the research is to narrow the gap of knowledge by re-examining the modified zone method in order to more accurately determine R-Values and U-Factors for CFS wall assemblies with whole wall framing factor percentages of 22% and above.
The research was focused on the three major structural elements of a typical cold-formed steel building - shear wall, floor joist, and column. Part 1 of the thesis explored wider options in the steel sheet sheathing for shear walls. An experimental research was conducted on 0.030 in and 0.033 in. (2:1 and 4:1 aspect ratios) and 0.027 in. (2:1 aspect ratio) steel sheet shear walls and the results provided nominal shear strengths for the American Iron and Steel Institute Lateral Design Standard. Part 2 of this thesis optimized the web hole profile for a new generation C-joist, and the web crippling strength was analyzed by finite element analysis. The results indicated an average 43% increase of web crippling strength for the new C-joist compared to the normal C-joist without web hole. To improve the structural efficiency of a cold-formed steel column, a new generation sigma (NGS) shaped column section was developed in Part 3 of this thesis. The geometry of NGS was optimized by the elastic and inelastic analysis using finite strip and finite element analysis. The results showed an average increment in axial compression strength for a single NGS section over a C-section was 117% for a 2 ft. long section and 135% for an 8 ft. long section; and for a double NGS section over a C-section was 75% for a 2 ft. long section and 103% for an 8 ft. long section.
Due to the accelerated growth in digital music distribution, it becomes easy to modify, intercept, and distribute material illegally. To overcome the urgent need for copyright protection against piracy, several audio watermarking schemes have been proposed and implemented. These digital audio watermarking schemes have the purpose of embedding inaudible information within the host file to cover copyright and authentication issues. This thesis proposes an audio watermarking model using MATLAB® and Simulink® software for 1K and 2K fast Fourier transform (FFT) lengths. The watermark insertion process is performed in the frequency domain to guarantee the imperceptibility of the watermark to the human auditory system. Additionally, the proposed audio watermarking model was implemented in a Cyclone® II FPGA device from Altera® using the Altera® DSP Builder tool and MATLAB/Simulink® software. To evaluate the performance of the proposed audio watermarking scheme, effectiveness and fidelity performance tests were conducted for the proposed software and hardware-in-the-loop based audio watermarking model.
The objective of this thesis was to develop an 8051 microcontroller soft core in the Verilog hardware description language (HDL). Each functional unit of the 8051 microcontroller was developed as a separate module, and tested for functionality using the open-source VHDL Dalton model as benchmark. These modules were then integrated to operate as concurrent processes in the 8051 soft core. The Verilog 8051 soft core was then synthesized in Quartus® II simulation and synthesis environment (Altera Corp., San Jose, CA, www.altera.com) and yielded the expected behavioral response to test programs written in 8051 assembler residing in the v8051 ROM. The design can operate at speeds up to 41 MHz and used only 16% of the FPGA fabric, thus allowing complex systems to be designed on a single chip. Further research and development can be performed on v8051 to enhance performance and functionality.
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