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 Degree Discipline: Engineering Technology
 Collection: UNT Theses and Dissertations
Synthesis of cubic boron nitride thin films on silicon substrate using electron beam evaporation.

Synthesis of cubic boron nitride thin films on silicon substrate using electron beam evaporation.

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Date: May 2004
Creator: Vemuri, Prasanna
Description: Cubic boron nitride (cBN) synthesis has gained lot of interest during the past decade as it offers outstanding physical and chemical properties like high hardness, high wear resistance, and chemical inertness. Despite of their excellent properties, every application of cBN is hindered by high compressive stresses and poor adhesion. The cost of equipment is also high in almost all the techniques used so far. This thesis deals with the synthesis of cubic phase of boron nitride on Si (100) wafers using electron beam evaporator, a low cost equipment that is capable of depositing films with reduced stresses. Using this process, need of ion beam employed in ion beam assisted processes can be eliminated thus reducing the surface damage and enhancing the film adhesion. Four sets of samples have been deposited by varying substrate temperature and the deposition time. scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray photoelectron spectroscopy (XPS), and Fourier transform infrared spectroscopy (FTIR) techniques have been used to determine the structure and composition of the films deposited. X-ray diffraction (XRD) was performed on one of the samples to determine the thickness of the film deposited for the given deposition rate. Several samples showed dendrites being formed as ...
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Effects of Thickness and Indenter Tip Geometry in Nanoindentation of Nickel Films

Effects of Thickness and Indenter Tip Geometry in Nanoindentation of Nickel Films

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Date: May 2004
Creator: Parakala, Padma
Description: Nanoindentation has become a widely used technique to measure the mechanical properties of materials. Due to its capability to deform materials in micro- and nano-scale, nanoindentation has found more applications in characterizing the deformation behavior and determining the mechanical properties of thin films and coatings. This research deals with the characterization of samples received from Center for Advanced Microstructures and Devices (CAMD) and Integran Technologies Inc., Toronto, Canada and the objective of this investigation was to utilize the experimental data obtained from nanoindentation to determine the deformation behavior, mechanical properties of thin films on substrates and bulk materials, and the effect of geometrically different indenters (Berkovich, cubecorner, and conical). X-ray diffraction (XRD), transmission electron microscope (TEM), scanning electron microscopy (SEM), and atomic force microscopy (AFM) analysis were performed on these materials to determine the crystal orientation, grain size of the material, and also to measure any substrate effects like pile-up or sin-in respectively. The results indicate that indentation size effect (ISE) strongly depends on shape of the indenter and less sensitive to penetration depth where as the hardness measurements depends on shape of indenter and depth of penetration. There is a negligible strain rate dependency of hardness at deeper depths ...
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Susceptibility of a digital turbine control system to IEEE 802.11 compliant emissions.

Susceptibility of a digital turbine control system to IEEE 802.11 compliant emissions.

Date: December 2003
Creator: Carter, Clinton E.
Description: Within the nuclear industry, there have been numerous instances of radio transmissions interfering with sensitive plant equipment. Instances documented vary from minor instrument fluctuations to major plant transients including reactor trips. With the nuclear power industry moving toward digital technologies for control and reactor protection systems, concern exists regarding their potential susceptibility to contemporary wireless telecommunications technologies. This study evaluates the susceptibility of Comanche Peak's planned turbine controls upgrade to IEEE 802.11 compliant wireless radio emissions. The study includes a review of previous research, industry emissions standards, and technical overview of the various IEEE 802.11 protocols and details the testing methodology utilized to evaluate the digital control system. The results of this study concluded that the subject digital control system was unaffected by IEEE 802.11 compliant emissions even when the transmitter was in direct contact with sensitive components.
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Linearity and monotonicity of a 10-bit, 125 MHz, segmented current steering digital to analog converter

Linearity and monotonicity of a 10-bit, 125 MHz, segmented current steering digital to analog converter

Date: May 2000
Creator: Bittle, Charles C.
Description: The purpose of this research is to determine the linearity and monotonicity of the THS5651IDW digital to analog converter (DAC), a prototype of the future Texas Instruments TLV5651, 10-bit, 125 MHz communication DAC. Testing was conducted at the Texas Instruments facility on Forest Lane, Dallas, Texas. Texas Instruments provided test equipment, software and laboratory space to obtain test data. Analysis of the data found the DAC to be monotonic since the magnitude of the differential nonlinearity (DNL) was less than ± 1 least significant bit (LSB) and the integral nonlinearity (INL) was less than ± 0.5 LSB. The study also showed that the DAC has primarily negative DNL although the DNL is well within the desired specification.
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Effect of engineered surfaces on valve performance.

Effect of engineered surfaces on valve performance.

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Date: December 2000
Creator: Pope, Larry G.
Description: Performance of air operated valves is a major maintenance concern in process industries. Anecdotal information indicates that reliability of some high maintenance valves has been improved by using an ion deposition process to achieve engineered surfaces on selected components. This project compared friction for various surface treatments of selected valve components. Results indicate valve performance may be slightly more consistent when an engineered surface is applied in the valve packing area; however surface treatment in this area does not appear to have a dominant affect on reducing valve friction. Results indicate a linear relation between stem friction and torque applied to packing flange nuts, and even after a valve is in service, controlled packing adjustments can be made without significantly changing valve stroke time.
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Effects of a surface engineered metallic coating on elastomeric valve stem seal leakage

Effects of a surface engineered metallic coating on elastomeric valve stem seal leakage

Date: December 2000
Creator: Taylor, John Abner
Description: Valve stem seal leakage is a major source of fugitive emissions, and controlling these emissions can result in added expense in leak detection and repair programs. Elastomeric O-rings can be used as valve stem seals, and O-ring manufacturers recommend lubrication of elastomeric seals to prevent damage and to assure proper sealing. In this research, a metallic coating was applied as a lubricant using a vacuum vapor deposition process to the surface of elastomeric valve stem seals. Valve stem leak measurements were taken to determine if the coated O-rings, alone or with the recommended lubrication, reduced valve stem seal leakage. This research determined that the metallic coating did not reduce valve stem leakage.
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A model for designing a new telecommunication system in Mongolia

A model for designing a new telecommunication system in Mongolia

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Date: May 2001
Creator: Baatarjav, Enkhbat
Description: The objective of this research is to design, and determine the feasibility of, a telecommunication system for the city of Erdenet, Mongolia. The Mongolian Telecommunication Company, Telecommunication Company of Erdenet city, and the National Statistical Office of Mongolia provided the data required for telecommunication forecasting of Erdenet. The literature review and analysis of the telecommunication forecasting indicate the need for a model of a new Telecommunication system in Erdenet, Mongolia. The model, as indicated, should become a useful example for planning and updating the telecommunication system in Mongolia. The design of a proposed telecommunication network involves the following considerations: analyzing and forecasting telephone traffic, calculating the required number of channels, determining exchange locations, traffic matrix, and establishing a basic hierarchical structure.
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Development of a Hybrid Molecular Ultraviolet Photodetector based on Guanosine Derivatives

Development of a Hybrid Molecular Ultraviolet Photodetector based on Guanosine Derivatives

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Date: December 2005
Creator: Liddar, Harsheetal
Description: Modern studies on charge transfer reaction and conductivity measurements of DNA have shown that the electrical behavior of DNA ranges from that of an insulator to that of a wide bandgap semiconductor. Based on this property of DNA, a metal-semiconductor-metal photodetector is fabricated using a self-assembled layer of deoxyguanosine derivative (DNA base) deposited between gold electrodes. The electrodes are lithographically designed on a GaN substrate separated by a distance L (50nm < L < 100nm). This work examines the electrical and optical properties of such wide-bandgap semiconductor based biomaterial systems for their potential application as photodetectors in the UV region wherein most of the biological agents emit. The objective of this study was to develop a biomolecular electronic device and design an experimental setup for electrical and optical characterization of a novel hybrid molecular optoelectronic material system. AFM results proved the usage of Ga-Polar substrate in conjugation with DG molecules to be used as a potential electronic based sensor. A two-terminal nanoscale biomolectronic diode has been fabricated showing efficient rectification ratio. A nanoscale integrated ultraviolet photodetector (of dimensions less than 100 nm) has been fabricated with a cut-off wavelength at ~ 320 nm.
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Characterization of boron nitride thin films on silicon (100) wafer.

Characterization of boron nitride thin films on silicon (100) wafer.

Date: August 2007
Creator: Maranon, Walter
Description: Cubic boron nitride (cBN) thin films offer attractive mechanical and electrical properties. The synthesis of cBN films have been deposited using both physical and chemical vapor deposition methods, which generate internal residual, stresses that result in delamination of the film from substrates. Boron nitride films were deposited using electron beam evaporation without bias voltage and nitrogen bombardment (to reduce stresses) were characterize using FTIR, XRD, SEM, EDS, TEM, and AFM techniques. In addition, a pin-on-disk tribological test was used to measure coefficient of friction. Results indicated that samples deposited at 400°C contained higher cubic phase of BN compared to those films deposited at room temperature. A BN film containing cubic phase deposited at 400°C for 2 hours showed 0.1 friction coefficient.
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Propagation analysis of a 900 MHz spread spectrum centralized traffic signal control system.

Propagation analysis of a 900 MHz spread spectrum centralized traffic signal control system.

Date: May 2006
Creator: Urban, Brian L.
Description: The objective of this research is to investigate different propagation models to determine if specified models accurately predict received signal levels for short path 900 MHz spread spectrum radio systems. The City of Denton, Texas provided data and physical facilities used in the course of this study. The literature review indicates that propagation models have not been studied specifically for short path spread spectrum radio systems. This work should provide guidelines and be a useful example for planning and implementing such radio systems. The propagation model involves the following considerations: analysis of intervening terrain, path length, and fixed system gains and losses.
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